Mild and Scalable Conditions for the Solvothermal Synthesis of Imine‐Linked Covalent Organic Frameworks
Andreas Laemont,
Gilles Matthys,
Roy Lavendomme
et al.
Abstract:A convenient method was developed that allows for the synthesis of highly crystalline and porous imine‐linked covalent organic frameworks (COFs) in hours. The use of an apolar solvent in combination with a precise amount of water and acetic acid was crucial to obtain materials of optimal quality. Fifteen different COFs could be produced under the same reaction conditions, using a green solvent mixture of n‐butanol, acetic acid and water at 70 °C for 16 hours with stirring. The crystallinity of the COFs produce… Show more
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