Abstraer. NMR experiments on high-T~ oxides done at Tokyo Metropolitan University are reviewed. The first is 89y NMR in YBCO with Y site dilutely substituted by Gd ions. The second is TE I of 63,65Cu NQR in YBCO. The third is 1H NMR from probe material coated on YBCO and BSCCO.In this article I would introduce NMR expe¡ on High-T c oxides done in our laboratories in the physics department of Tokyo Metropolitan UniversityThe first work is a 89y NMR by Sakamoto et al. [1] which was made on a standard High-Tc oxide of YBCO (Te-92 K) with Y site dilutely substituted by Gd ions. In the earlier stage of high-Te studies, one of apparently mysterious phenomena was that the Te was not reduced by the substitution of Y site by the magnetic rare earth ions, which was in contrast with the sharp reduction of T c in the conventional super conducting substances. That observation impfied that the magnetic coupling is so weak between the Y site and CuO2 planes carrying the superconducting current. Our work was undertaken to elucidate the magnetic coupling between Y site and the CuO2 planes. The observed induction decay rates at 100 K were analyzed by the RKKY interactions. The result was that the exchange coupling constant J between the Y site and the CuO2 plane is less than J=< 0.01 eV. This value is compared with J = 0.3 eV for Gd atoms in Ag metal, for example.The second work is the transverse relaxation rates T21 of Cu NQR in the YBCO. In a course of precise temperature dependence experiment, Tei et al.[2-4] discovered a sharp peak of T21 at 35 K for the superconducting plane site Cu(2). The finding was independently made by Russian workers. A lot of interest has been paid to this anomaly concerning with the mechanism of high-T~ oxides. The extraordinarily sharp profile of the peak strongly sug-