Modification of polyhedral oligomeric silsesquioxane derivatives with heck reaction as possible new bio-hybrid materials

Günkara, Ömer Tahir

doi:10.1080/10426507.2019.1576678

Phosphorus, Sulfur, and Silicon and the Related Elements

2019

DOI: 10.1080/10426507.2019.1576678

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Modification of polyhedral oligomeric silsesquioxane derivatives with heck reaction as possible new bio-hybrid materials

Ömer Tahir Günkara

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2020

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Synthesis of nanofibers organosiloxane structures under hydrothermal conditions

Черкашина

Pavlenko

Samoilova

et al. 2020

IOP Conf. Ser.: Mater. Sci. Eng.

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The paper presents the possibility of producing polyhedral oligomeric silsesquioxanes (POSS) under hydrothermal conditions in a high-pressure reactor. POSS was prepared by hydrolytic polycondensation of cyclohexyl trichlorosilane under conditions of elevated temperature and pressure. Morphology and structure of the final products were characterized by X-ray diffraction (XRD), thermal analysis (TGA and DTA) in an atmosphere of argon, Fourier transform infrared spectrum (FT-IR) and scanning electron micrograph (SEM). The resulting compound is a nanofibers of a polyhedral oligomeric silsesquioxane. The diameter of the obtained nanofibers is 50 … 150 nm, and the length is from 200 nm to 30 μm.

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Synthesis of nanofibers organosiloxane structures under hydrothermal conditions

Черкашина

Pavlenko

Samoilova

et al. 2020

IOP Conf. Ser.: Mater. Sci. Eng.

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show abstract

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Modification of polyhedral oligomeric silsesquioxane derivatives with heck reaction as possible new bio-hybrid materials

Cited by 1 publication

References 46 publications

Synthesis of nanofibers organosiloxane structures under hydrothermal conditions

Synthesis of nanofibers organosiloxane structures under hydrothermal conditions

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