Morphology control of amino acid particles in interfacial crystallization using inkjet nozzle

Crystallization Behavior of Glycine Molecules with Electrolytic Dissociation on Charged Silica Gel Particles

“…The crystal structure of glycine was investigated by powder X‐ray diffraction (PXRD) (RINT‐2000; Rigaku Corporation, Tokyo, Japan) with Cu K α ( λ = 0.15406 nm) at a voltage of 40 kV and a current of 200 mA. The mass fraction of α ‐glycine in the solid phase was calculated by …”

Change in glycine polymorphs induced by minute-bubble injection during antisolvent crystallisation

“…The polymorphs of the product glycine were identified by X-ray diffraction (XRD, RINT-2100, Rigaku Co.), and the selectivity of polymorphs was determined using the XRD peaks at 2h = 15°for the a-form, 18°for the b-form, and 21°for the c-form [16][17][18]. The XRD peak intensity ratio of the a-form reflection to the b-form or c-form for the corresponding concentration ratio in the range 0/100% a-form in b-form or c-form was a linear function [16].…”

Mutual diffusion diagram of liquid-liquid interfaces for morphological control of NaCl crystals

“…Because this method does not require thermal energy and can suppress supersaturation fluctuations by limiting the crystal precipitation field to the liquid-liquid interface, it could be applied to a wide range of materials. We have controlled crystal morphology by changing parameters such as organic solvent species, contact time, and solute concentration [18][19][20], and we have prepared composite particles from multicomponent solutions [21]. Therefore, this method may be suitable for producing particles instead of crystallization methods such as evaporation, cooling, and anti-solvent addition.…”