2016
DOI: 10.1002/celc.201600449
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Nanoparticle Surface Coverage Controls the Speciation of Electrochemically Generated Chlorine

Abstract: Cyclic voltammetry is used to investigate the oxidation of chloride on platinum nanoparticles. The electrochemical response of the nanoparticles drop‐cast onto a glassy carbon electrode is compared to that recorded at a platinum macroelectrode. The use of “nano”‐ and “macro”‐scale Pt reveals different ratios of the electrochemically formed products, chlorine (Cl2) and the trichloride (Cl3−) anion. This difference in the speciation is attributed to the chloride oxidation being a surface‐reaction‐limited process… Show more

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