NanoXAS—The in situ Combination of Scanning Transmission X-ray and Scanning Probe Microscopy

Schmid, I.; Raabe, Jörg; Wenzel, Sabine; Fink, R.; Hug, H. J.; Quitmann, C.; McNulty, Ian; Eyberger, Catherine; Lai, Barry

doi:10.1063/1.3625399

AIP Conference Proceedings

2011

DOI: 10.1063/1.3625399

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NanoXAS—The in situ Combination of Scanning Transmission X-ray and Scanning Probe Microscopy

I. Schmid¹,

Jörg Raabe²,

Sabine Wenzel³

et al.

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Cited by 2 publications

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A hot tip: imaging phenomena using in situ multi-stimulus probes at high temperatures

Nonnenmann

2016

Nanoscale

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Accurate high temperature characterization of materials remains a critical challenge to the continued advancement of various important energy, nuclear, electronic, and aerospace applications. Future experimental studies must assist these communities to progress past empiricism and derive deliberate, predictable designs of material classes functioning within active, extreme environments. Successful realization of systems ranging from fuel cells and batteries to electromechanical nanogenerators and turbines requires a dynamic understanding of the excitation, surface-mediated, and charge transfer phenomena which occur at heterophase interfaces (i.e. vapor-solid, liquid-solid, solid-solid) and impact overall performance. Advancing these frontiers therefore necessitates in situ (operando) characterization methods capable of resolving, both spatially and functionally, the coherence between these complex, collective excitations, and their respective response dynamics, through studies within the operating regime. This review highlights recent developments in scanning probe microscopy in performing in situ imaging at high elevated temperatures. The influence of and evolution from vacuum-based electron and tunneling microscopy are briefly summarized and discussed. The scope includes the use of high temperature imaging to directly observe critical phase transition, electronic, and electrochemical behavior under dynamic temperature settings, thus providing key physical parameters. Finally, both challenges and directions in combined instrumentation are proposed and discussed towards the end.

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A hot tip: imaging phenomena using in situ multi-stimulus probes at high temperatures

Nonnenmann

2016

Nanoscale

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X-ray Absorption Spectroscopy: An Indispensable Tool to Study Single-Atom Catalysts

Wang

Yan

2020

Synchrotron Radiation News

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NanoXAS—The in situ Combination of Scanning Transmission X-ray and Scanning Probe Microscopy

Cited by 2 publications

References 6 publications

A hot tip: imaging phenomena using in situ multi-stimulus probes at high temperatures

A hot tip: imaging phenomena using in situ multi-stimulus probes at high temperatures

X-ray Absorption Spectroscopy: An Indispensable Tool to Study Single-Atom Catalysts

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