2019
DOI: 10.3390/app9163406
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NMR Relaxometry and IR Thermography to Study Ancient Cotton Paper Bookbinding

Abstract: Defects related to degradation were observed in an ancient book paperboard cover through nuclear magnetic resonance relaxometry and infrared thermography. Data collected with this combined method allowed identifying areas with moisture content and thermal diffusivity anomalies within the front board, corresponding to the different conservation status of the cellulose-based material. Non-destructive testing analytical procedures provide comprehensive knowledge for preserving precious library archives.

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Cited by 9 publications
(4 citation statements)
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References 31 publications
(44 reference statements)
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“…In the study of ancient books, PT has been applied to the analysis of bookbinding and, more specifically, to the investigation of the adhesion state among their different parts [ 37 ] and/or to the detection of the presence of possible damage [ 38 ]. Such experiments have often been carried out by means of integrated approaches combining the use of PT with other techniques able to provide complementary results, such as near-infrared reflectography (NIR) [ 39 ], and two-dimensional proton nuclear magnetic resonance relaxometry [ 40 , 41 ].…”
Section: Pt And/or Passive Irt Applicationsmentioning
confidence: 99%
“…In the study of ancient books, PT has been applied to the analysis of bookbinding and, more specifically, to the investigation of the adhesion state among their different parts [ 37 ] and/or to the detection of the presence of possible damage [ 38 ]. Such experiments have often been carried out by means of integrated approaches combining the use of PT with other techniques able to provide complementary results, such as near-infrared reflectography (NIR) [ 39 ], and two-dimensional proton nuclear magnetic resonance relaxometry [ 40 , 41 ].…”
Section: Pt And/or Passive Irt Applicationsmentioning
confidence: 99%
“…A different kind of damage has been investigated by Sfarra et al (2018) using an integrated approach by IRT and other analyses which included chemical tests, to obtain a map of the book´s structural elements and the characterization of defects in a historical bookbinding. NIR and IRT were employed together to explore the bookbinding elements while two-dimensional proton nuclear magnetic resonance relaxometry (NMR) was applied to reveal the chemical composition of the bookbinding (Sfarra et al 2018;Tortora, Sfarra, and Casieri 2019).…”
Section: Subsurface Structural Elements In Bindingsmentioning
confidence: 99%
“…Moreover, IRT detects subsurface features in artworks and locates their position . Nowadays, IRT has become one of the most effective methods for the analysis of books (Mercuri et al 2015), making it possible to characterize structural elements of bookbinding (Mercuri et al 2011;Sfarra et al 2018;Tortora, Sfarra, and Casieri 2019), the adhesion of gildings in illuminated manuscripts (Doni et al 2014), and biological damage in parchment (Mercuri, Pinzari et al 2018). In particular, IRT has been applied to detect underdrawings in illuminations ), text buried inside bookbindings (Mercuri, Gnoli et al 2013), and erased graphical features from archival documents (Loreti et al 2016).…”
Section: Introductionmentioning
confidence: 99%
“…PT, one of the photo-thermal techniques used for the evaluation of different thermal parameters in several materials [18,19], has been employed to investigate different kinds of artefacts [20][21][22][23][24][25], enabling the study of both optically opaque samples, such as bronzes [26][27][28][29][30], and semi-transparent materials [31,32], such as paintings [33][34][35][36] and books [37]. In particular, it has been proven to be very effective for the study of ancient codices, enabling the non-destructive characterization of the main features of both book bindings [37][38][39] and illuminations [40,41]; in addition, it is used for the evaluation of the state of conservation of the books. Moreover, PT has been used to reveal subsurface graphical elements underlying illuminations, such as underdrawings and pentimenti [40].…”
Section: Introductionmentioning
confidence: 99%