Novel Cellulosic Natural Fibers from Abelmoschus Ficulneus Weed: Extraction and Characterization for Potential Application in Polymer Composites

Ramalingam, Karthikeyan; Thiagamani, Senthil Muthu Kumar; Pulikkalparambil, Harikrishnan; Muthukumar, Chandrasekar; Krishnasamy, Senthilkumar; Siengchin, Suchart; Alosaimi, Abeer M.; Hussein, Mahmoud A.; Rangappa, Sanjay Mavinkere

doi:10.1007/s10924-022-02687-9

Cited by 20 publications

(4 citation statements)

References 53 publications

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“…The density of the filler was also determined during the investigation. Standard procedures were followed for this evaluation per our preceding reports [ 66 , 67 , 68 ].…”

Section: Methodsmentioning

confidence: 99%

Characterization of Syzygium cumini (L.) Skeels (Jamun Seed) Particulate Fillers for Their Potential Use in Polymer Composites

Thiagamani,

Yaswanth,

Yashwanth

et al. 2024

Molecules

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Syzgium cumini (L.) Skeels powder (S. cumini powder), also known as Jamun, is well-known for its various medical and health benefits. It is especially recognized for its antidiabetic and antioxidant properties. Thus, S. cumini powder is used in various industries, such as the food and cosmetic industries. In this work, the fruit of S. cumini was utilized; its seeds were extracted, dried, and ground into powder. The ground powders were subjected to various techniques such as physicochemical tests, Fourier transform infrared (FTIR) spectroscopy, X-ray diffractometry (XRD), particle size analysis, scanning electron microscopy (SEM), energy-dispersive X-ray spectroscopy (EDX), thermogravimetric analysis (TGA), differential scanning calorimetry (DSC), and antioxidant analysis. From the physicochemical tests, it was revealed that the jamun seed filler contained cellulose (43.28%), hemicellulose (19.88%), lignin (23.28%), pectin (12.58%), and wax (0.98%). The FTIR analysis supported these results. For instance, a peak at 2889 cm−1 was observed and associated with CH stretching, typically found in methyl and methylene groups, characteristic of cellulose and hemicellulose structures. The XRD results demonstrated that the crystallinity index of the jamun seed filler was 42.63%. The particle analysis indicated that the mean (average) particle size was 25.34 μm. This observation was ensured with SEM results. The EDX spectrum results showed the elemental composition of the fillers. Regarding thermal degradation, the jamun seed filler had the ability to withstand temperatures of up to 316.5 °C. Furthermore, endothermic and exothermic peaks were observed at 305 °C and 400 °C, respectively. Furthermore, the antioxidant property of the powder displayed a peak scavenging activity of 91.4%. This comprehensive study not only underscores the viability of S. cumini powder as a sustainable and effective particulate filler in polymer composites but also demonstrates its potential to enhance the mechanical properties of composites, thereby offering significant implications for the development of eco-friendly materials in various industrial applications.

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“…The density of the filler was also determined during the investigation. Standard procedures were followed for this evaluation per our preceding reports [ 66 , 67 , 68 ].…”

Section: Methodsmentioning

confidence: 99%

Characterization of Syzygium cumini (L.) Skeels (Jamun Seed) Particulate Fillers for Their Potential Use in Polymer Composites

Thiagamani,

Yaswanth,

Yashwanth

et al. 2024

Molecules

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“…stem [12] Waltheria indica L. stem [13] Furcraea selloa K Koch peduncle [14] Sapodilla Seed [8] Abelmoschus ficulneus [19] Senna auriculata [20] Cellulose (wt%) 40.…”

Section: Constituents Btar Fillermentioning

confidence: 99%

Isolation and characterization of banyan tree root filler for polymer composites in light-weight applications

Sivaram R,

Thiagamani,

Khan

et al. 2024

Mater. Res. Express

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The applicability of bio fillers as reinforcement with polymers is promoted by cost- and environmentally-conscious concerns. Nowadays, a large range of reinforcements are employed for this purpose, including cellulosic fillers and natural fibres owing to the favorable mechanical behavior, minimal price, negligible tool wear, low density, and eco-friendliness etc. The main purpose of the investigation is to explore the possibilities of utilizing plant sources as reinforcing filler in polymeric matrices. In this study particulate fillers were obtained from banyan tree’s aerial roots and were subjected to various characterization such as physiochemical evaluation, Fourier Transform Infrared Spectroscopy (FTIR), X-ray diffraction (XRD), thermal analysis (TGA), and Scanning Electron Microscopy (SEM). From the physiochemical analysis it was found that the banyan tree aerial root filler (BTAR) contained 40.13% of Cellulose, 15.22% of Hemicellulose, 15.31% of Lignin and 6.86% of Pectin. The density of the BTAR filler was found as 0.27 kg/cc whereas average particle size was 136.3 µm. The maximum inflection temperature referred to the maximum degradation of the BTAR filler was 295.7oC. The SEM analysis exposed the rough surface of filler, with micro-structured strands and pores. The rough surface and the pores could help in better bond ability of the matrix and reinforcement when combined. With these properties the BTAR filler could be a potential candidate as a strengthening material for polymers in different light weight applications.

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“…Crystalline and amorphous fibre characteristics differ between parts of the tree and between trees. Previous studies suggested that fibres with fewer amorphous contents such as hemicellulose, lignin and pectin possess better mechanical properties [ 82 , 83 ].…”

Section: Natural Fibres In Packagingmentioning

confidence: 99%

“…Composites reinforced with chemically treated natural fibres generally show enhanced mechanical properties because of improved interfacial adhesion between the fibre and the matrix [ 82 ]. Numerous surface treatment methods are available for the modification of natural fibres.…”

Section: Physical and Chemical Modifications Of Fibres For Food Packa...mentioning

confidence: 99%

Recent Advances in Natural Fibre-Based Materials for Food Packaging Applications

et al. 2023

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Packaging is one of the major domains in the food processing industry that reduces waste and enhances product shelf life. Recently, research and development have focused on bioplastics and bioresources to combat environmental issues caused by the alarming growth of single-use plastic waste food packaging. The demand for natural fibres has recently increased because of their low cost, biodegradability and eco-friendliness. This article reviewed recent developments in natural fibre-based food packaging materials. The first part discusses the introduction of natural fibres in food packaging, with a focus on fibre source, composition and selection parameters, while the second part investigates the physical and chemical ways to modify natural fibres. Several plant-derived fibre materials have been utilised in food packaging as reinforcements, fillers and packaging matrices. Recent investigations developed and modified natural fibre (physical and chemical treatments) into packaging using casting, melt mixing, hot pressing, compression moulding, injection moulding, etc. These techniques majorly improved the strength of bio-based packaging for commercialisation. This review also identified the main research bottlenecks and future study areas were suggested.

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Novel Cellulosic Natural Fibers from Abelmoschus Ficulneus Weed: Extraction and Characterization for Potential Application in Polymer Composites

Cited by 20 publications

References 53 publications

Characterization of Syzygium cumini (L.) Skeels (Jamun Seed) Particulate Fillers for Their Potential Use in Polymer Composites

Characterization of Syzygium cumini (L.) Skeels (Jamun Seed) Particulate Fillers for Their Potential Use in Polymer Composites

Isolation and characterization of banyan tree root filler for polymer composites in light-weight applications

Recent Advances in Natural Fibre-Based Materials for Food Packaging Applications

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