“…Two unbound resonances have been observed in 24 O above the one-neutron separation energy [19,23,24], and there is also evidence for resonances above the two-neutron separation energy [19,23] around 7.5 MeV. The first tentative evidence that one of these resonances decays by sequential emission of two neutrons was deduced from a measurement of two discrete neutron energies in coincidence similar to a γ-ray cascade [23]. In this Rapid Communication we present the first observation of a twoneutron sequential decay, exposed by energy and angular correlations, in 24 O.…”