Oligosaccharide-based quality evaluation of Atractylodis rhizome and a strategy for simplifying its quality control

Zhuang, Dan; Qin, Jing; Wang, Huiyang; Yi, Zhang; Liu, Chun-yao; Ding, Qin; Lv, Guangping

doi:10.1186/s13065-019-0605-8

Cited by 15 publications

(9 citation statements)

References 28 publications

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“…Lin et al (2010) reported RSD of 2.59-11.43% for intra-day and 7.12-11.9% for inter-day precision in LC-MS inulin quantification. Similar results were reported in the study of Zhuang et al (2019) where they obtained intra-day precision of 0.29-4.43% and inter-day precision of 5.74-10.91% for three different concentrations (n = 6), and accuracy of 83.16-99.6% (n = 3) in HPLC-ELSD analysis of inulin-type fructooligosaccharides.…”

Section: Repeatability and Reproducibilitysupporting

confidence: 89%

Inulin Determination by an Improved HPLC-ELSD Method

et al. 2021

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Since inulin utilization as a sugar or fat replacer, texture modifier, and emulsifier is increasing in the food industry, there is a need for its determination for food control and labeling. This study reports the development and validation of an advanced high-performance liquid chromatographic method with evaporative light-scattering detection (HPLC-ELSD) method for inulin quantification, with optimized extraction conditions (1:10 w/v solid-to-solvent ratio, 1 h/80 °C in a water bath continued with 30 min ultrasonication for the extraction step, and precipitation during the night with four volumes of acetone). The rapid HPLC-ELSD analysis (16 min) has been performed by isocratic elution with water as a mobile phase and optimized detector parameters (temperature of evaporator 80 °C, temperature of nebuliser 80 °C, gas flow rate 1.3 standard liters per minute, detector gain 1). The method was validated in terms of limits of detection and quantification, intra-and inter-day precision and accuracy, and recovery. The proposed method was carried out using a cation exchange (Ag +) column for the first time for the inulin determination, avoiding the hydrolysis step in order to simplify and accelerate the quantification.

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Section: Repeatability and Reproducibilitysupporting

confidence: 89%

Inulin Determination by an Improved HPLC-ELSD Method

et al. 2021

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“…Множество гликозидных связей и трудности экстракции для получения ОС с ненарушенной структурой препятствуют развитию технологий химического синтеза аналитических стандартов высокомолекулярных ОС. В поисках выхода из сложившейся ситуации изучаются возможности извлечения и очистки стандартов ОС в аналитических лабораториях с помощью твердофазной экстракции, высокоэффективной жидкостной хроматографии (HPLC) или их комбинации [37]. Так, например, Li et al [38] извлекли и очистили стандарты КОС (степень полимеризации 2-6; чистота > 99%) с использованием твердофазной экстракции с последующей хроматографией гидрофильного взаимодействия (HILIC).…”

Section: особенности контроля олигосахаридовunclassified

“…Данные Zhuang et al [37] подтверждают более высокую чувствительность HPLC-ELSD по сравнению с HPLC-RID, а также стабильность исходного уровня благодаря совместимости с градиентным элюированием и независимости от температуры. Последующие работы исследователей позволили увеличить чувствительность метода.…”

Section: методы количественной оценки олигосахаридовunclassified

The practice of application and features of the control of oligosaccharides in the production of specialized food products. A review

Yurova

Ananyeva

2023

Food systems

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Functional oligosaccharides include various groups of carbohydrates with the biological activity — an ability to modulate gut microbiota due to the prebiotic, anti-adhesive and anti-inflammatory activities. The unique properties of oligosaccharides explain a wide spectrum of their use in the dairy industry: from food ingredients for imitation of the prebiotic activity of human milk oligosaccharides in infant dry milk mixtures to structuring additives, replacers of sugar and fat. When choosing oligosaccharides for inclusion into dairy products, their biological activity and technological properties that depend on a source and method for extraction of these compounds are assessed. Fructooligosaccharides, galactooligosaccharides, xylooligosaccharides and pectic oligosaccharides have been most widely used. When developing recipes of products with stated biological effectiveness, it is necessary to remember that consumption of large amounts of substances with prebiotic properties can lead to the gastrointestinal disorder, which requires introducing into practice the control of the oligosaccharide quantitative content in the product composition. The aim of this review is analysis of possibilities of using oligosaccharides in production of specialized milk-based food products and methods for controlling quality, safety and effectiveness of inclusion of such products into a diet. The review considers the existing methods for quantitative identification of oligosaccharides included in the composition of dairy products as functional ingredients. The emphasis is made on the limitations of the introduction of the developed analytical methods into routine practice of the oligosaccharide control, which is linked with the complexity and multicomponent nature of the food matrix under study. The necessity of the further improvement of methods for quantitative identification of functional oligosaccharides in foods is shown.

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“…The branch chain consists of →3, 5)-Araf-(1→, →5)-Araf-(1→, and Araf-(1→. A series of oligo-saccharides DP 3-15 were separated from A. lancea and identified as FOS, which consisted of linear β-(2, 1)-linked fructofuranosyl units mostly carry a terminal single α-(1–2)-linked α-glucopyranosyl unit ( Zhuang et al, 2019 ). The ACPS was extracted via ultrasonic method in enzymolysis A. lancea.…”

Section: Phytochemistrymentioning

confidence: 99%

Atractylodis Rhizoma: A review of its traditional uses, phytochemistry, pharmacology, toxicology and quality control

Zhang

Zhao

Chang

et al. 2021

Journal of Ethnopharmacology

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Ethnopharmacological relevance Atractylodis Rhizoma (AR), mainly includes Atractylodes lancea (Thunb.) DC. ( A. lancea ) and Atractylodes chinensis (DC.) Koidz. ( A. chinensis ) is widely used in East Asia as a diuretic and stomachic drug, for the treatment of rheumatic diseases, digestive disorders, night blindness, and influenza as it contains a variety of sesquiterpenoids and other components of medicinal importance. Aim of the review A systematic summary on the botany, traditional uses, phytochemistry, pharmacology, toxicology, and quality control of AR was presented to explore the future therapeutic potential and scientific potential of this plant. Materials and methods A review of the literature was performed by consulting scientific databases including Google Scholar, Web of Science, Baidu Scholar, Springer, PubMed, ScienceDirect, CNKI, etc. Plant taxonomy was confirmed to the database “The Plant List”. Results Over 200 chemical compounds have been isolated from AR, notably sesquiterpenoids and alkynes. Various pharmacological activities have been demonstrated, especially improving gastrointestinal function and thus allowed to assert most of the traditional uses of AR. Conclusions The researches on AR are extensive, but gaps still remain. The molecular mechanism, structure-activity relationship, potential synergistic and antagonistic effects of these components need to be further elucidated. It is suggested that further studies should be carried out in the aspects of comprehensive evaluation of the quality of medicinal materials, understanding of the “effective forms” and “additive effects” of the pharmacodynamic substances based on the same pharmacophore of TCM, and its long-term toxicity in vivo and clinical efficacy.

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Oligosaccharide-based quality evaluation of Atractylodis rhizome and a strategy for simplifying its quality control

Cited by 15 publications

References 28 publications

Inulin Determination by an Improved HPLC-ELSD Method

Inulin Determination by an Improved HPLC-ELSD Method

The practice of application and features of the control of oligosaccharides in the production of specialized food products. A review

Atractylodis Rhizoma: A review of its traditional uses, phytochemistry, pharmacology, toxicology and quality control

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