“…Yet several interesting aspects of dealloyed materials are still subject of contemporary research, such as the structural stability and coarsening behavior of the ensuing nanoporous structures 17 or their mechanical properties. 18 A broad variety of in situ methods have been utilized to study the dealloying process itself, ranging from dilatometry, 19 resistometry, 20 magnetometry, 21 UV–vis spectroscopy, 22 transmission X-ray microscopy (XTM), 23 X-ray diffraction (XRD), 24 − 26 and Raman spectroscopy 27 to real-space imaging techniques such as scanning tunneling microscopy 28 and transmission electron microscopy (TEM). 29 While microscopic techniques, in general, allow the extraction of size information for the nanoporous structures, they suffer from the disadvantage of averaging over a limited sample area only.…”