On the mechanism of reaction of ε-caprolactam with phosphorous chlorides

Rakhimov, A. I.; Pugacheva, E. A.

doi:10.1134/s1070363208010088

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2013

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“…In fact, triethylamine started to be used rather long time ago as a HCl acceptor not only for reaction of phosphorochloridite with amines per se, but also for reactants with the -NH-C(O)-group, such as N-methylacetamide [13,14].…”

Section: Methodsmentioning

confidence: 99%

Synthesis of intermediate compounds with P-N bond from (thio)carbamates and chlorodioxaphospholanes and -phosphorinanes and their reactivity

Murzin

Kolesova

2013

Eur. J. Chem.

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KEYWORDSA variety of 2-(N-alkoxy(thio)carbonyl alkyl(aryl)amino)-1,3,2-dioxaphospholanes and phosphorinanes were prepared from chlorodioxaphospholanes and phosphorinanes. Their structures were determined by IR, Mass and NMR spectroscopy. These compounds were employed in direct reactions with elemental sulphur and methylester of chloroacetic acid giving potentially physiologically active N-phosphorylated carbamates with P(O)-N and P(S)N bonds.

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Section: Methodsmentioning

confidence: 99%