One step hydrothermal synthesis and characterization of moss like MWCNT-Bi2S3 nanomaterial for solid phase extraction of copper

Memon, Zainab Manzoor; Yılmaz, Erkan; Soylak, Mustafa

doi:10.1016/j.talanta.2017.06.068

Cited by 14 publications

(7 citation statements)

References 58 publications

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“…It also plays a role in the ionization degree of the adsorbent. 28 Therefore, the column was first conditioned at different pH values in the range of 1 -10. Then, model solutions (25 mL of solutions containing 50 μg Ni(II)) were prepared and conditioned at different pH values in the range of 1 -10, respectively.…”

Section: Ph Effectmentioning

confidence: 99%

Separation and Preconcentration of Nickel(II) from Drinking, Spring, and Lake Water Samples with Amberlite CG-120 Resin and Determination by Flame Atomic Absorption Spectrometry

et al. 2018

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In this study, Amberlite CG-120 adsorbent was used for the separation/preconcentration of Ni(II) ions in commercial drinking, spring and lake water samples before detection by flame atomic absorption spectrometry. Various optimization parameters for Ni(II) determination, such as pH, eluent type and concentration, sample and eluent flow rates, amount of adsorbent, were investigated to obtain better sensitivity, accuracy, precision and quantitative recovery. Furthermore, the interference effects of some ions on the recovery efficiency of Ni(II) were also investigated. The optimum experimental parameters were obtained in the case of pH 1; 5 mL of 4 mol L-1 HCl for eluent and 0.3 g for the adsorbent amount. The limit of detection was found to be 0.58 μg L-1 and linearity ranged from 5 to 50 μg L-1. The accuracy of the method was tested by the certified reference material of TMDA-70.2 Ontario Lake Water at a 95% confidence level.

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Section: Ph Effectmentioning

confidence: 99%

Separation and Preconcentration of Nickel(II) from Drinking, Spring, and Lake Water Samples with Amberlite CG-120 Resin and Determination by Flame Atomic Absorption Spectrometry

et al. 2018

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show abstract

“…Among the various treatment technologies, adsorption is currently preferred as a non-hazardous method for the removal of heavy metal ions due to its cheapness, selectivity, high efficiency, simple processes, reusability, flexibility in design and availability of different adsorbents 11 . Generally, an ideal adsorbent should have a high surface area and also adsorption sites, so that the adsorption process takes place in a short equilibrium time 11 , 12 . In the last two decades, by the development of novel nanotechnologies and the advent of nanomaterials 13 , 14 , scientists have been attracted to this field and various novel adsorbents have been emerged 15 .…”

Section: Introductionmentioning

confidence: 99%

Effective removal of Pb(II) ions using piperazine-modified magnetic graphene oxide nanocomposite; optimization by response surface methodology

Alboghbeish

Larki

Saghanezhad

2022

Sci Rep

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In this research, the piperazine-modified magnetic graphene oxide (Pip@MGO) nanocomposite was synthesized and utilized as a nano-adsorbent for the removal of Pb(II) ions from environmental water and wastewater samples. The physicochemical properties of Pip@MGO nanocomposite was characterized by X-ray diffraction analysis (XRD), Field emission scanning electron microscopy (FESEM), Transmission electron microscopy (TEM), Energy-dispersive X-ray spectroscopy (EDAX), Thermo-gravimetric analysis (TGA), Vibrating Sample Magnetometery (VSM) and Fourier-transform infrared spectroscopy (FT-IR) analysis. In this method, the batch removal process were designed by response surface methodology (RSM) based on a central composite design (CCD) model. The results indicated that the highest efficiency of Pb(II) removal was obtained from the quadratic model under optimum conditions of prominent parameters (initial pH 6.0, adsorbent dosage 7 mg, initial concentration of lead 15 mg L−1 and contact time 27.5 min). Adsorption data showed that lead ions uptake on Pip@MGO nanocomposite followed the Langmuir isotherm model equation and pseudo-second order kinetic model. High adsorption capacity (558.2 mg g−1) and easy magnetic separation capability showed that the synthesized Pip@MGO nanocomposite has great potential for the removal of Pb(II) ions from contaminated wastewaters.

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“…Among the various treatment technologies, adsorption is currently preferred as a non-hazardous method for the removal of heavy metal due to its cheapness, selectivity, high efficiency, simple processes, reusability, flexibility in design and availability of different adsorbents 10 . Generally, an ideal adsorbent should have a high surface area and also adsorption sites, so that the adsorption process takes place in a short equilibrium time 10,11 .…”

Section: Introductionmentioning

confidence: 99%

Piperazine-modified magnetic graphene oxide (Pip@MGO) as a novel nanocomposite for the effective removal of lead ions; using RSM optimization

Alboghbeish

Saghanezhad

Larki

2022

Preprint

View full text Add to dashboard Cite

In this research, the piperazine-modified magnetic graphene oxide (Pip@MGO) nanocomposite was synthesized and utilized as a nano-adsorbent for the removal of Pb(II) ions from environmental water and wastewater samples. The physicochemical properties of Pip@MGO nanocomposite was characterized by XRD, FESEM, TEM, EDX, TGA, VSM and FT-IR analysis. In this method, the batch removal process were designed by response surface methodology (RSM) based on a central composite design (CCD) model. The results indicated that the highest efficiency of Pb(II) removal was obtained from the quadratic model under optimum conditions of prominent parameters (initial pH: 6.0, adsorbent dosage: 7 mg, initial concentration of lead: 15 mg L− 1 and contact time: 27.5 min). Adsorption data showed that lead ions uptake on Pip@MGO nanocomposite followed the Langmuir isotherm model equation and pseudo-second order kinetic model. High adsorption capacity (558.2 mg g− 1) and easy magnetic separation capability showed that the synthesized Pip@MGO nanocomposite has great potential in removal of Pb(II) ions from contaminated wastewaters.

show abstract

One step hydrothermal synthesis and characterization of moss like MWCNT-Bi2S3 nanomaterial for solid phase extraction of copper

Cited by 14 publications

References 58 publications

Separation and Preconcentration of Nickel(II) from Drinking, Spring, and Lake Water Samples with Amberlite CG-120 Resin and Determination by Flame Atomic Absorption Spectrometry

Separation and Preconcentration of Nickel(II) from Drinking, Spring, and Lake Water Samples with Amberlite CG-120 Resin and Determination by Flame Atomic Absorption Spectrometry

Effective removal of Pb(II) ions using piperazine-modified magnetic graphene oxide nanocomposite; optimization by response surface methodology

Piperazine-modified magnetic graphene oxide (Pip@MGO) as a novel nanocomposite for the effective removal of lead ions; using RSM optimization

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