Operationally simple enzymatic deprotection of C-3 position on 3,4,6-tri-O-acetyl-d-glucal

Zamysłowski, Tomasz; Gorczyca, Katarzyna; Zhang, Yuqing; Poterała, Marcin; Malinowski, Maciej

doi:10.1016/j.carres.2023.108848

Carbohydrate Research

2023

DOI: 10.1016/j.carres.2023.108848

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Operationally simple enzymatic deprotection of C-3 position on 3,4,6-tri-O-acetyl-d-glucal

Tomasz Zamysłowski,

Katarzyna Gorczyca,

Yuqing Zhang

et al.

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2024

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Selective Carbohydrate Deacetylation: Simple and Mild Approach based on Supported Copper Nanoparticles

Marchán‐García,

Lo Fiego,

Moglie

2024

Helvetica Chimica Acta

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Herein, a selective protocol for the complete removal of acetyl protecting groups from carbohydrate derivatives based on copper nanoparticles supported on activated carbon is presented. The deacetylation procedure occurs under neutral conditions, is applicable to a wide range of substrates and tolerates a variety of functional groups (e.g. azido, allyl and silyl groups). Quantitative yields of the deacetylated product were obtained for all evaluated derivatives using catalyst amounts between 1 and 10 mol%. As a special highlight, the dual behavior of the nanocatalyst in both deacetylation and click reactions is reported.

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Selective Carbohydrate Deacetylation: Simple and Mild Approach based on Supported Copper Nanoparticles

Marchán‐García,

Lo Fiego,

Moglie

2024

Helvetica Chimica Acta

View full text Add to dashboard Cite

show abstract

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Operationally simple enzymatic deprotection of C-3 position on 3,4,6-tri-O-acetyl-d-glucal

Cited by 1 publication

References 36 publications

Selective Carbohydrate Deacetylation: Simple and Mild Approach based on Supported Copper Nanoparticles

Selective Carbohydrate Deacetylation: Simple and Mild Approach based on Supported Copper Nanoparticles

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