(1) Depending on tools and fabrication parameters, surface structures may be quite different, even though their roughness is in the same range (here ±0.6 µm).(2) Depending on the surface structure, more or less cavities remain after diffusion welding at low pressure (1050°C, 25 Mpa, 2 h) with vacuum sealing. Remaining cavities at the weld interface lead to reduced Charpy properties. But weld defects may be restored by applying a second high pressure HIP step (1050°C, 100 Mpa, 2 h) without vacuum sealing. (3) Charpy properties after 1, 2, 3, and 14 days surface oxidation at humid air (before welding at 1150°C, 25 MPa, 2 h). After 2 days oxidation in humid air DBTT is clearly deteriorated. However, there is no loss of upper shelf energy, but some severe scattering results have been observed, even for the reference fabrication process.
Surface Fabrication Study
Surface Contamination Study(4) Charpy properties after different wetting and cleaning procedures (before welding at 1150°C, 25 MPa, 2 h). Best results are achieved after milling with coolant and cleaning with isopropanol. Furthermore, oil is obviously not a useful protector against oxidation.(5) The micrographs of all weld interfaces show now weld line. That is, from a micro-structural point of view the diffusion welds (peformed at 1150°C, under 25 MPa, for 2 hours) are all perfect, regardless of the fabrication history. The above shown Charpy test results, however, demonstrate that there are differences, anyway.