2022
DOI: 10.1016/j.ultsonch.2022.105954
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Optimized ultrasound-assisted extraction of phenolic compounds from Thymus comosus Heuff. ex Griseb. et Schenk (wild thyme) and their bioactive potential

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Cited by 31 publications
(49 citation statements)
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“…The UHPLC was based on the utilization of a Waters BEH C18 column (2.1 × 100 mm, 1.7 μm). The mass spectrometry conditions were adapted from a previously published work [ 22 ]. Briefly, the flow rate was 200 μL/min; the injection volume was 6 μL; the full scan MS-data-dependent (Top n = 3) MS/MS mode was used for ion acquisition in the range 80–1200 m/z , with a positive ionization mode and a mass resolution of 70,000 FWHM.…”
Section: Methodsmentioning
confidence: 99%
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“…The UHPLC was based on the utilization of a Waters BEH C18 column (2.1 × 100 mm, 1.7 μm). The mass spectrometry conditions were adapted from a previously published work [ 22 ]. Briefly, the flow rate was 200 μL/min; the injection volume was 6 μL; the full scan MS-data-dependent (Top n = 3) MS/MS mode was used for ion acquisition in the range 80–1200 m/z , with a positive ionization mode and a mass resolution of 70,000 FWHM.…”
Section: Methodsmentioning
confidence: 99%
“…For TEAC, an ABTS + radical solution was prepared by reacting 7 mM ABTS solution with 2.45 mM potassium persulfate, and then the mixture was left in the dark at room temperature for 12–16 h. The ABTS+ radical solution was diluted until an absorbance of 0.70 ± 0.02 at 734 nm, and then 200 μL of radical solution were added to 20 μL of the sample (at a 1 mg/mL concentration). After 30 min of incubation in the dark at room temperature, the absorbances were read at 734 nm, and the results were expresses as milligrams of Trolox equivalents per g of freeze-dried powder (mg TE/g dw) [ 21 , 22 ].…”
Section: Methodsmentioning
confidence: 99%
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