2024
DOI: 10.1021/acs.joc.3c02175
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Organophosphorus-Catalyzed Direct Dehydroxylative Thioetherification of Alcohols with Hypervalent Organosulfur Compounds

Gang Sun,
Shi-Ping Zhan,
Yi-Feng Zhao
et al.

Abstract: A metal-free and thiol-free organophosphoruscatalyzed method for forming thioethers was disclosed, driven by P III /P V �O redox cycling. In this work, one-step dehydroxylative thioetherification of alcohols was fulfilled with various hypervalent organosulfur compounds. This established strategy features an excellent functional group tolerance and broad substrate scope, especially inactivated alcohols. The scale-up reaction and further transformation of the product were also successful. Additionally, this meth… Show more

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