2024
DOI: 10.1021/acsorginorgau.4c00028
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Parallel Minisci Reaction of gem-Difluorocycloalkyl Building Blocks

Serhii Holovach,
Illia Poroshyn,
Kostiantyn P. Melnykov
et al.

Abstract: Parallel Minisci reactions of nonfluorinated and gem-difluorinated C4–C7 cycloalkyl building blocks (trifluoroborates and carboxylic acids) with a series of electron-deficient heterocycles were studied. A comparison of the reaction’s outcome revealed better product yields in the case of carboxylic acids as the radical precursors in most cases, albeit these reagents were used with three-fold excess under optimized conditions. The nature of the heterocyclic core was found to be important for successful incorpora… Show more

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