A significant improvement has been made in the identification of γ rays from muon capture in natural Ca, and to a lesser extent for Fe and Ni. For calcium, capture was observed in 44 Ca and even 42 Ca, as well as the dominant 40 Ca. The (µ − , ν) reaction was clearly observed in 40 Ca, but, as in the past, no clear identification was made in Fe and Ni. The (µ − , νn) reaction was clearly observed in all nuclei, and the γ rays observed correspond better to the (γ, p) reaction than to spectroscopic factors from the (d, 3 He) or (t, α) reactions. Some (µ − , ν2n) and other reactions have been observed at a lower yield.