Particle Size and Humidity Effects on Nanocellulose Adhesion to Glass: Implications for Mitigating Particulate Contamination in Industrial Processes

Abstract

Particulates adhered to glass surfaces can result in manufacturing defects during display module fabrication. The adhesion force is highly sensitive to the water meniscus formed in humid environments and can be examined experimentally as a function of relative humidity using atomic force microscopy by measuring the pull-off force between a flat glass surface and either a spherical or a cone-shaped probe tip. In this work, the effective thickness and hydrogen bonding interaction of adsorbed water were probed using transmission FTIR at Brewster's angle with p-polarized light, investigating two different multicomponent glass surfaces subject to different aqueous treatments. The effective thickness of water layers so measured was used to estimate the curvature of the water meniscus at the particulate−glass interface, thereby enabling the prediction of the adhesion forces exerted on the nanoparticles and microspheres in pull-off measurements. Correlations between the adsorbed water layer, the electrostatic charging, and the adhesion force of cellulosic materials to glass from the nanoscale to the microscale are discussed in this work, which provide insights into mitigating particulate contamination in industrial processes.

Water Adsorption Isotherm and Surface Conductivity of Boroaluminosilicate Glasses

“…27 Moreover, the surface charge electrostatically attracts particles to the glass surface during manufacture or fabrication. 6,28 Such adhesion of airborne particles can cause interference with the alignment of structural patterns and device failure leading to overall yield loss. 24−26 Therefore, understanding the charging mechanisms of flat panel display-type glasses is important because it can help identify strategies for minimizing or eliminating surface charging, which can ultimately lead to improved device performance and yield.…”

“…Glass surface science is of significant importance in both academic research − and industrial development − of various physical and chemical processes including aqueous corrosion, − crack/flaw generation/propagation, − and particle adhesion. ,, Flat panel display industries use glass substrates for thin-film transistors on panel devices in which electrostatic charging can directly impact downstream manufacturing. − Process problems associated with surface charging have grown more challenging in recent years due to decreasing pixel dimensions of ultrahigh-density displays . Moreover, the surface charge electrostatically attracts particles to the glass surface during manufacture or fabrication. , Such adhesion of airborne particles can cause interference with the alignment of structural patterns and device failure leading to overall yield loss. − Therefore, understanding the charging mechanisms of flat panel display-type glasses is important because it can help identify strategies for minimizing or eliminating surface charging, which can ultimately lead to improved device performance and yield.…”

“…Glass surface science is of significant importance in both academic research 1−6 and industrial development 7−11 of various physical and chemical processes including aqueous corrosion, 12−16 crack/flaw generation/propagation, 17−21 and particle adhesion. 6,22,23 Flat panel display industries use glass substrates for thin-film transistors on panel devices in which electrostatic charging can directly impact downstream manufacturing. 24−26 Process problems associated with surface charging have grown more challenging in recent years due to decreasing pixel dimensions of ultrahigh-density displays.…”