A novel portable particulate matter measuring system was designed, developed and qualified. The heavy-duty engine Federal Test Procedure (FTP) requires the use of a full-flow tunnel to measure particulate emissions from diesel fueled engines. However, a full-flow tunnel based constant volume sampler (CVS) system is not only expensive to build and maintain, it also requires a large work space. The portable micro-dilution system that could be used for measuring on-board, in-use emissions from heavy-duty vehicles would cost significantly less. The micro-dilution tunnel operates on the same principle as a full-flow dilution tunnel. The added advantage of the proposed design is that unlike a full-flow tunnel, dilution ratios can be controlled very accurately. The micro-dilution tunnel system was designed to maintain a dilution ratio of at least four to one. Dilution ratios were determined by measuring the mass flow rates of the dilution air and dilute exhaust, and the difference of the two was equal to the raw exhaust mass flow rate. The design incorporates a novel (3.175 mm in diameter, and 0.254 m long) concentric stainless dilution tunnel, which was a porous stack sampler manufactured by Mott Corporation. The unique feature of the system is its use of a single pump for not only drawing the diluted exhaust out of the micro-dilution tunnel, but also supplying filtered and dry dilution air to the tunnel. The system was used to collect PM emissions data from two different engines, namely, Navistar T444E and Detroit Diesel Series 60. The engines were tested over several steady state and transient tests. The micro-dilution system was compared to West Virginia University's (WVU) Engine and Emissions Research Laboratory (EERL) full flow tunnel system. As expected, the particulate matter data correlated better with steady state than with transient tests. The particulate matter mass emission rates were within 14% for the steady state tests and within 17% for majority of the transient tests of the full-flow laboratory's PM mass emissions data. However, one transient test resulted in a 33% difference between the micro-dilution tunnel and the full-flow dilution tunnel. The test results indicate that modifications are necessary to the micro-dilution system before it is to be used for on-road PM emission measurements. iii ACKNOWLEDGEMENTS As my sixth year at West Virginia University comes to an end, I must say that all goods things must come to an end. There are several people who have played an important role during my graduate studies at WVU and I would like to try to thank each and every one of them. I must first thank Dr. Mridul Gautam for giving me the opportunity to attend graduate school. Thank you for being my advisor and friend. Your support has encouraged me to keep going and never give up. I also wish to thank my other committee members, Dr. Gary Morris and Dr. Greg Thompson for their continued support and influence throughout my graduate education. I would like to thank the most important people in my life, my family....