Numerous analytical methods are available for analyzing beryllium: inductively coupled plasma‐mass spectrometry (ICP‐MS), optical emission spectrometry (ICP‐OES), atomic absorption spectrometry (AAS), colorimetric, and fluorimetric methods (10, 11). A detailed listing of the colorimetric methods can be found in Taylor et al. (12). The preferred method for soil and water analysis in the environmental business is ICP‐MS following United States Environmental Protection Agency (USEPA) methods 200.7 and 6010. The ICP‐MS instrumentation has greater sensitivity and reduced interference from other metals, compared to other analytical methods. A typical reporting limit of beryllium in environmental investigations using the ICP‐MS method is 5 ppb; typical method of detection limits for soil and water are 0.1 µg/kg and 0.7 µg/L, respectively. AAS is also an USEPA approved process following method 7090 or 7091. Due to beryllium's low concentration and subsequent interference with other metals in environmental samples, a number of separation and preconcentration methods have been developed using chelating agents, ion‐exchange resins, sorbants, and surfactants.