Phosphorylation of pyridoxal azomethines. Synthesis of phosphorus containing azomethines and furopyridines

Пудовик, М. А.; Kibardina, L. K.; Trifonov, A. V.; Dobrynin, Alexey B.; Katsyuba, Sergey A.; Бурилов, А. Р.

doi:10.1080/10426507.2018.1513516

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2022

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“…Azomethines are precursors for the synthesis of new compounds with valuable properties. For example, O-phosphorylated derivatives of pyridoxal, a vitamin involved in biochemical processes, were prepared using azomethines [15].…”

Section: Introductionmentioning

confidence: 99%

Crystallization of Nano-Sized Macromolecules by the Example of Hexakis-[4-{(N-Allylimino)methyl}phenoxy]cyclotriphosphazene

2022

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The synthesized compound was characterized by 31P, 13C, and 1H NMR spectroscopy and MALDI-TOF mass spectroscopy. According to DSC data, the compound was initially crystalline, but the crystal structure was defective. The crystals suitable for X-ray diffraction study were prepared by slow precipitation of the compound from a solution by a vapor of another solvent. A study of the single crystal obtained in this way demonstrated that the phosphazene ring has a flattened chair conformation. It was found that the sphere circumscribed around the compound molecule has a diameter of 2.382 nm.

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Section: Introductionmentioning

confidence: 99%