Perovskite material is a material with chemical formula ABX 3 -type, which exhibits a similar crystal structure of CaTiO 3 . In this material, A and B are metal cations with ionic valences combined to +6, e.g., Li + :Nb 5+ ; Ba 2+ :Ti 4+ ; Sr 2+ :Mn 4+ ; La 3+ :Fe 3+ , and X is an electronegative anion with ionic valence (−2), such as O 2− , S 2− , etc. The properties of a perovskite material strongly depend on the synthesis route of materials. The perovskite materials may be oxides (ABO 3 :CaMnO 3 ), halides (ABX 3 : X = Cl, Br, I), nitrides (ABN 3 :CaMoN 3 ), sulfides (ABS 3 :LaYS 3 ), etc., and they may exist in different forms, such as powders, thin films, etc. There are various routes for the synthesis of several perovskites, such as solid-state synthesis, liquid-state synthesis, gas-state synthesis, etc. In this chapter, we discuss various techniques for the synthesis of oxide perovskites in powder form using solid-, liquid-, and gas-state synthesis methods, and we also present an overview on the other type of perovskite materials. The X-ray diffraction, scanning electron microscopy, and optical techniques are used to study the purity of crystallographic phase, morphology, and photoluminescence properties of the perovskite materials. Some applications of different perovskite materials are also discussed.