Background: Mineral trioxide aggregate (MTA), is commonly used in endodon9c and re--stora&ve procedures. Objec&ve: Our objec&ve was to introduce gas adsorp&on porosimetry as a viable method for evalua1on of general porosity and specific pore characteris1cs of set Portland cement used in subs1tute for MTA, to inves1gate the effect of two different obtu--ra#on methods (compac#on and compac#on in conjunc#on with indirect ultrasonic agita--!on of the cement paste), and to evaluate the correla.on between the specific pore char--acteris(cs to compressive strength in general. Material and Methods: Portland cement samples were prepared and divided into two groups based on compac4on techniques. An ini#al stereomicroscopic evalua*on was done to assess any differences in appearance of pores randomly selected from either of the two experimental groups. Specific pore charac--teris&cs and compressive strength werequan&fied by a gas adsorp&on porosimeter and an Instron universal tes(ng machine. A two--tailed student t--test was used for sta,s,cal com--parison of data, and a regression analysis was done to evaluate the correla6on between each specific pore characteris-c and compressive strength in general. Results: The gas po--rosimetry method provided measurable values rela2ng to specific pore characteris2cs of Portland cement. The stereomicroscopy evalua6on revealed marked differences between samples from the two groups, namely visibly larger pores both on the outside surface and in cross--sec$ons of specimens prepared by the indirect ultrasonic ac$va$on method. Con--clusions: Gas adsorp*on porosimetry is a feasible method for evalua*on of specific pore characteris)cs of Portland cement and poten)ally other dental materials as well.