BACKGROUNDPre‐treatment of plant materials is essential in producing plant‐based products and can affect their various organoleptic and physicochemical characteristics. This work aimed to study the effect of pre‐treatment of vegetable raw materials, namely, ultrasonic processing, and freezing of raw materials under various low‐temperature conditions to obtain multiple types of vegetable milk and determine their characteristics.RESULTSIt is shown that by applying a certain kind of pre‐treatment of vegetable raw materials, it is possible to adjust organoleptic parameters and the content of solids, protein, fat, carbohydrates, fiber, and mineral composition of various types of vegetable milk from soy, rice, oats, wheat, peas, buckwheat, pumpkin seeds, lentils. Ultrasound pre‐treatment allows increasing polyphenol content by an average of 15‐20% for all types of plant milk, except for lentil milk. The results showed that ultrasound treatment for 3 minutes had the most significant effect on the overall acceptability for lentils, pumpkin, rice, and pea milk. Pre‐freezing at a temperature regime of ‐17°C and ‐85°C contributed to an increase in Fe, K, Zn, Ca, Mg, Si, and P by an average of 30 to 100%, depending on the plant material.CONCLUSIONPre‐treatment of vegetable raw materials, including freezing and ultrasonic treatment, can positively affect the macro‐ and micronutrient composition of plant milk. However, the effect may vary depending on the type of raw material and processing conditions.This article is protected by copyright. All rights reserved.