Increasing traffic requires durable and low-noise road surfaces. Urban residents complain about excessive traffic noise that leads to an unhealthy environment. Understanding techniques to produce durable, low-noise pavement has led to the development of rubberized concrete block pavement (RCBP) and rubberized asphalt concrete pavement (RACP). The chapter examines morphology and chemical properties of waste tyre rubber using FESEM, XRF, and TGA/DTA.