Preparation and application of a fortified hair reference material for the determination of methamphetamine and amphetamine

Lee, Sooyeun; Park, Yonghoon; Han, Eunyoung; Choe, Sanggil; Lim, Mi Ae; Chung, Heesun

doi:10.1016/j.forsciint.2008.04.005

Cited by 26 publications

(11 citation statements)

References 24 publications

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“…Amphetamines and related compounds have usually been extracted from urine samples by liquid-liquid extraction (LLE) [17][18][19], supercritical fluid extraction (SFE) [20], solid-phase extraction (SPE) [21,22], and solid-phase microextraction (SPME) [23][24][25]. However, there are several disadvantages of conventional extraction procedures such as LLE and SPE.…”

Section: Introductionmentioning

confidence: 99%

Solid-phase extraction followed by dispersive liquid-liquid microextraction for the sensitive determination of ecstasy compounds and amphetamines in biological samples

Mashayekhi¹,

Rezaee²,

Khalilian³

2014

Bull. Chem. Soc. Eth.

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ABSTRACT. A novel approach for the determination of ecstasy and amphetamines (3,4-methylenedioxymethylamphetamine (MDMA, Ecstasy), 3,4-methylenedioxyamphetamine (MDA), 3,4-methylenedioxyethylamphetamine (MDEA) and 3,4-methylenedioxypropylamphetamine (MDPA)) in biological samples is presented. The analytes were extracted from the matrix and transferred to a small volume of a high density, water insoluble solvent using solid-phase extraction (SPE) followed by dispersive liquid-liquid microextraction (DLLME). This combination not only resulted in a high enrichment factor, but also it could be used in complex matrices (biological samples). Some important extraction parameters, such as sample solution flow rate, sample pH, type and volume of extraction and disperser solvents as well as the salt addition, were studied and optimized. Under the optimized conditions, the calibration graphs were linear in the range of 0.5-500 µg L -1 and 1.0-500 µg L -1 with detection limits in the range of 0.1-0.3 µg L -1 and 0.2-0.7 µg L -1 in urine and plasma samples, respectively. The results showed that SPE-DLLME is a suitable method for the determination of ecstasy components and amphetamines in biological and water samples.

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Section: Introductionmentioning

confidence: 99%

Solid-phase extraction followed by dispersive liquid-liquid microextraction for the sensitive determination of ecstasy compounds and amphetamines in biological samples

Mashayekhi¹,

Rezaee²,

Khalilian³

2014

Bull. Chem. Soc. Eth.

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“…Quality assurance issues in forensic hair analysis have also been reported in some papers [13][14][15][16]. In particular, we previously reported the evaluation of measurement uncertainty (MU) for methamphetamine (MA) and its metabolite, amphetamine (AP), in hair [17][18][19][20] and urine [21] in the field of forensic science.…”

Section: Introductionmentioning

confidence: 96%

Establishment of the measurement uncertainty of 11-nor-D9-tetrahydrocannabinol-9-carboxylic acid in hair

Han

Yang

Lee

et al. 2011

Forensic Science International

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“…Therefore, several methods, such as gas chromatography (GC), 3,4 high performance liquid chromatography (HPLC), 5 GC-mass spectrometry (MS), [6][7][8][9][10][11][12] HPLC-MS, 13,14 capillary electrophoresis (CE), 15 and CE-MS, 16 along with sample preparation methods have been developed for the determination of amphetamine and related compounds at low concentration in biological matrices. In order to eliminate interferences from the biological matrices, liquid-liquid extraction (LLE), [17][18][19] supercritical fluid extraction (SFE), 20 solid-phase extraction (SPE), 21,22 and solid-phase microextraction (SPME) [23][24][25] have been proposed. However, there are several disadvantages for conventional extraction procedures such as LLE and SPE.…”

Section: Introductionmentioning

confidence: 99%

Mixed-Hemimicelle Solid Phase Extraction Followed by Dispersive Liquid-Liquid Microextraction of Amphetamines from Biological Samples

Khalilian¹,

Rezaee²

2016

Journal of the Brazilian Chemical Society

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In this work, the synthesized Fe 3 O 4 nanoparticles was coated by sodium dodecyl sulfate and then it was used as a sorbent in mixed-hemimicelle solid phase extraction of some amphetamines, as psychoactive drugs, from biological samples. This extraction method was combined with dispersive liquid-liquid microextraction to enhance enrichment factors of targeted analytes. Effect of different parameters influencing the hybrid extraction performance, such as sodium dodecyl sulfate amount and sample pH, were investigated. The method showed linearity in the range of 1.0-250 and 2.0-250 µg L -1 for the most of analytes in urine and plasma samples, respectively. The limits of detection, based on signal to noise of 3, were found 0.1-0.2 and 0.3-0.5 µg L -1 in urine and plasma samples, respectively. The results of the intra-day and inter-day precision were less than 13.5% for all amphetamines. The amounts of relative recoveries in spiked urine and plasma samples were found in the range of 90-96 and 87-93%, respectively.

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Preparation and application of a fortified hair reference material for the determination of methamphetamine and amphetamine

Cited by 26 publications

References 24 publications

Solid-phase extraction followed by dispersive liquid-liquid microextraction for the sensitive determination of ecstasy compounds and amphetamines in biological samples

Solid-phase extraction followed by dispersive liquid-liquid microextraction for the sensitive determination of ecstasy compounds and amphetamines in biological samples

Establishment of the measurement uncertainty of 11-nor-D9-tetrahydrocannabinol-9-carboxylic acid in hair

Mixed-Hemimicelle Solid Phase Extraction Followed by Dispersive Liquid-Liquid Microextraction of Amphetamines from Biological Samples

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