Preparation and Photochemistry of 3-O-Methylestra-1,3,5(10)-Triene-17beta-yl Cinnamates and 3-O-Methylestra-1,3,5(10)-Trien-17-one O-Cinnamoyl-17-Oximes

Azani, Mariam Al; Graham, John; Thiemann, Thies

doi:10.3390/ecsoc-18-a039

Proceedings of the 18th International Electronic Conference on Synthetic Organic Chemistry 2014

DOI: 10.3390/ecsoc-18-a039

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Preparation and Photochemistry of 3-O-Methylestra-1,3,5(10)-Triene-17beta-yl Cinnamates and 3-O-Methylestra-1,3,5(10)-Trien-17-one O-Cinnamoyl-17-Oximes

Mariam Al Azani

John Graham

Thies Thiemann

Abstract: 17-oxime, respectively, in the presence of PPh 3 -CBrCl 3 in an Appel-type reaction. Under photolysis, the steroidal cinnamates underwent E-/Z-isomerization, while the steroidal Ocinnamoyloximes underwent E-/Z-isomerization concomitant with cleavage reactions.

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Preparation and Photochemistry of 3-O-Methylestra-1,3,5(10)-Triene-17beta-yl Cinnamates and 3-O-Methylestra-1,3,5(10)-Trien-17-one O-Cinnamoyl-17-Oximes

Abstract: 17-oxime, respectively, in the presence of PPh 3 -CBrCl 3 in an Appel-type reaction. Under photolysis, the steroidal cinnamates underwent E-/Z-isomerization, while the steroidal Ocinnamoyloximes underwent E-/Z-isomerization concomitant with cleavage reactions.

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References 15 publications

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