2009
DOI: 10.1007/s11771-009-0031-5
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Preparation and sintering of nano Fe coated Si3N4 composite powders

Abstract: Fe/Si 3 N 4 composite powder was synthesized by the heterogeneous precipitation-thermal reduction process, and then pressed into flakes under a pressure of 10 MPa. Flakes were sintered by pressureless and hot-pressing at 1 600 ℃ under 0.1 MPa N 2 . The chemical composition, phases and microstructure of composite powder and sintered flakes were investigated by energy dispersive spectroscopy (EDS), X-ray diffraction (XRD), scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The results… Show more

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Cited by 4 publications
(2 citation statements)
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“…The theory of minimum energy and the minimum rate of energy dissipation have been applied to flow around bluff bodies, stability of falling bodies, statics and dynamics of gas bubbles, generation of ripples and dunes, and drag reduction by suspended load. These examples are used to illustrate how the minimization principles (variational principles) can be used to solve the problems of dissipative mechanical systems in static or dynamic equilibrium conditions [8,9,10,11]. In Ref.…”
Section: The Least Energy Consumption Principlementioning
confidence: 99%
“…The theory of minimum energy and the minimum rate of energy dissipation have been applied to flow around bluff bodies, stability of falling bodies, statics and dynamics of gas bubbles, generation of ripples and dunes, and drag reduction by suspended load. These examples are used to illustrate how the minimization principles (variational principles) can be used to solve the problems of dissipative mechanical systems in static or dynamic equilibrium conditions [8,9,10,11]. In Ref.…”
Section: The Least Energy Consumption Principlementioning
confidence: 99%
“…At present, the collaborative effect of metal Fe, Mo coated Si 3 N 4 and the generation Si 3 N 4 whisker on the mechanism of toughening has not been reported. Despond on our preliminary works [8] , we got the Fe-Mo/Si 3 N 4 composite powders by use the heterogeneous precipitation-thermal reduction synthesis, and the Fe-Mo/Si 3 N 4 composite powders sintered by normal pressing in N 2 atmosphere in different sintering temperatures. During preparation process of the powders, sintering densification, microstructure evolution, and strengthening mechanisms of Fe-Mo/Si 3 N 4 cermets have been investigated in different temperatures to provide a theoretical guidance to obtain the best sintering temperature of Fe-Mo/Si 3 N 4 cermets with high mechanical properties.…”
Section: Introductionmentioning
confidence: 99%