Preparation of Ag-Pd Alloy Particles by Ultrasonic Spray Pyrolysis and Application to Electrode for LTCC

Abstract

Spherical Ag-Pd alloy particles were prepared from aqueous solutions of AgNO 3 and Pd NO 3 2 by ultrasonic spray pyrolysis. As-prepared powders were dense and non-agglomerated particles, which had sub-micron size and narrow size distribution. XRD shows that as-prepared particles are polycrystalline and the crystal phase of the as-prepared particles has an alloy composition. Ag-Pd particles obtained from spray pyrolysis offer superior oxidation-resistivity of Pd as compared with those obtained from coprecipitation.

Sintering and Dielectric Properties of Ba(Mg_1/3Ta_2/3)O₃ Particle Prepared by Spray Pyrolysis

“…This result suggests that the particle size distribution of the as-prepared powders is relatively narrow. Thus far, we have obtained a similar result in the synthesis of Ag-Pd alloy powders by spray pyrolysis [11]. TEM observation revealed that an average size of the BMT nano-particles was around 20 nm, and that these particles were aggregated.…”

Effect of gas environment on the properties of silver–glass composite powders with core–shell structure prepared by spray pyrolysis

“…Kang). ders [8][9][10][11][12]. However, metal-glass composite powders have not been studied well because of the different preparation process of metal and glass powders.…”

Characteristics of nano-sized silver–glass composite powders prepared by flame spray pyrolysis

“…However, nano-sized glass powders for silver conducting films have not been well developed. Metal-metal and metal-ceramic composite powders have been extensively studied to improve the properties of pure metal powders [15][16][17][18]. However, metal-glass composite powders have not been studied well because of the different preparation process of metal and glass powders.…”