Preparation of aluminum alkoxide by ethylene glycol

Seri, Osami; Tanno, Satoshi

doi:10.2464/jilm.59.424

J.JILM

2009

DOI: 10.2464/jilm.59.424

|View full text |Cite

Preparation of aluminum alkoxide by ethylene glycol

Osami Seri¹,

Satoshi Tanno²

Abstract: Aluminum ethyleneglycoxides, Al OCH 2 CH 2 OH 3 were obtained when aluminum powder mixed with AlCl 3 has been refluxed in dehydrated ethylene glycol at 471 K for 12 h. Characteristics of the aluminum ethyleneglycoxide were measured by XRD and particle size distribution analysis. Particle morphology observed by SEM was like rectangular column shape. It is considered that the aluminum ethyleneglycoxides obtained is interpreted as corrosion product which is a reaction product that aluminum was corroded in ethylen… Show more

Help me understand this report

Search citation statements

Order By: Relevance

Paper Sections

Select...

Citation Types

Supporting

Mentioning

Contrasting

Year Published

2010

2014

Publication Types

Select...

Article5

Relationship

Self Cite0

Independent5

Authors

Journals

Cited by 5 publications

References 4 publications

Supporting

Mentioning

Contrasting

Order By: Relevance

Preparation of alumina particles through corrosion product of aluminum in methanol

Seri¹,

Sasaki²

2010

J.JILM

View full text Add to dashboard Cite

It was found that coupons of aluminum can material 5182 were corroded in dehydrated methanol with aluminum chloride. The higher solution temperature was, the more rapidly dissolution occurred. It is shown that similar pattern of XRD analysis, particle size distribution analysis and particle morphology observation revealed that corrosion product of 5182 coincided with aluminumtrimethoxide supplied in commercial market when they were hydrolyzed and then calcinated. The 5182 dissolution product was electrochemically interpreted as corrosion product which is aluminumtrimethoxide oxidized in methanol containing aluminum chloride as catalyst.

show abstract

Preparation of alumina particles through corrosion product of aluminum in methanol

Seri¹,

Sasaki²

2010

J.JILM

View full text Add to dashboard Cite

show abstract

Preparation of alumina powder by phenol solvent

Seri¹,

Hisanobu²

2010

J.JILM

View full text Add to dashboard Cite

Aluminum has been dissolved by corrosion approach making use of phenol as a solvent and aluminum chloride as a catalyst for a period of 2.1 ks refluxing process. White aluminum oxide powder was successfully obtained when the solution has been hydrated and dried in electric oven. The powder derived from our approach above was evaluated in comparison with aluminumphenoxide reagent. When the powder was sintered at 1473 K for 3.6 ks, the apparent a-alumina was confirmed by XRD analysis, which showed completely same XRD patterns of the aluminumphennoxide reagent. It was found that the shape of our a-alumina powder was a few micron meter size hexagonal scales. From electrochemical point of view, the dissolution of aluminum in phenol was explained as the corrosion phenomena of aluminum.

show abstract

Preparation of CoAl2O4 by Corrosion Synthesis

Seri¹,

Iwama²,

Sasaki³

2013

J. Jpn. Soc. Powder Powder Metallurgy

View full text Add to dashboard Cite

scite is a Brooklyn-based organization that helps researchers better discover and understand research articles through Smart Citations–citations that display the context of the citation and describe whether the article provides supporting or contrasting evidence. scite is used by students and researchers from around the world and is funded in part by the National Science Foundation and the National Institute on Drug Abuse of the National Institutes of Health.

Contact Info

customersupport@researchsolutions.com

10624 S. Eastern Ave., Ste. A-614

Henderson, NV 89052, USA

This site is protected by reCAPTCHA and the Google Privacy Policy and Terms of Service apply.

Blog Terms and Conditions API Terms Privacy Policy Contact Cookie Preferences Do Not Sell or Share My Personal Information

Made with 💙 for researchers

Part of the Research Solutions Family.

Preparation of aluminum alkoxide by ethylene glycol

Cited by 5 publications

References 4 publications

Preparation of alumina particles through corrosion product of aluminum in methanol

Preparation of alumina particles through corrosion product of aluminum in methanol

Preparation of alumina powder by phenol solvent

Preparation of CoAl2O4 by Corrosion Synthesis

Contact Info

Product

Resources

About