Preparation of high purity carbonyl[<sup>35</sup>S]sulphide

Kluczewski, S.M.; Brown, Keith A.; Bell, J.N.B.; Sandalls, F.J.; Jones, Brian M.; Minski, M.J.

doi:10.1002/jlcr.2580210510

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Cited by 6 publications

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“…K3'S was synthesised in a glass vessel similar to that of Kluczewski et uI(1984) [4] (Fig 1 .), but this was enlarged to give a higher overall yield as the gas was to be used far *Author to whom correspondance should be sent. containing 17 mg d' sulphur in toluene.…”

Section: Methodsmentioning

confidence: 99%

The preparation of high purity H₂³⁵S

Collins¹,

Bell²

1994

Labelled Comp Radiopharmac

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Section: Methodsmentioning

confidence: 99%

The preparation of high purity H₂³⁵S

Collins¹,

Bell²

1994

Labelled Comp Radiopharmac

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Sulfur Compounds

Weil¹,

Sandler²

2000

Kirk-Othmer Encyclopedia of Chemical Technology

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Sulfur is a component of many compounds. Carbon sulfides, thiophosgenes, trichloromethanesulfenyl chloride, hydrogen sulfide, hydrogen polysulfides (sulfanes), sulfur halides and oxyhalides, sulfur nitrides, sulfur oxides, sulfur oxygen acids and their salts, thiocyanic acid and its salts, methanesulfonyl chloride, and methanesulfonic acid are all discussed, along with properties, manufacture, shipment and storage, economic aspects, analytical methods, grades and specifications, health and safety, and uses.

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Sulfur Compounds

Weil¹,

Sandler²,

Gernon³

2006

Kirk-Othmer Encyclopedia of Chemical Technology

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Sulfur is a component of many industrially useful compounds, particularly process intermediates. Other sulfur compounds are important because of air pollution considerations, coming from natural sources (COS, SO 2 , H 2 S) as well as manmade. Carbon sulfides, carbonyl sulfide, thiophosgene, trichloromethanesulfenyl chloride, hydrogen sulfide, hydrogen polysulfides (sulfanes) and their salts, sulfur halides and oxyhalides, sulfur nitrides, sulfur oxides, sulfur oxygen acids and their salts, thiocyanic acid and its salts, methanesulfonyl chloride, and methanesulfonic acid are all discussed, along with properties, manufacture, shipment and storage, economic aspects, analytical methods, grades and specifications, health and safety, and uses in making agricultural pesticides, pharmaceuticals, food chemicals, oil additives, plastics and plastic additives, and refining catalysts. Elemental sulfur, sulfuric acid, sulfur trioxide, carbon disulfide, thiosulfates and sulfur removal from natural gas are discussed in separate articles in this Encyclopedia .

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Preparation of high purity carbonyl[³⁵S]sulphide

Abstract: SUMMARYThe title compound was synthesised by the reaction between elementary[ 35S]sulphur and carbon monoxide at 3OO0C, and purified by passage over Porapak QS. <0.05% (v/v) of the COS concentration.The only detectable S-impurity i n the purified product was C S g at

Cited by 6 publications

References 4 publications

The preparation of high purity H₂³⁵S

The preparation of high purity H₂³⁵S

Sulfur Compounds

Sulfur Compounds

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Preparation of high purity carbonyl[35S]sulphide

Abstract: SUMMARYThe title compound was synthesised by the reaction between elementary[ 35S]sulphur and carbon monoxide at 3OO0C, and purified by passage over Porapak QS. <0.05% (v/v) of the COS concentration.The only detectable S-impurity i n the purified product was C S g at

Cited by 6 publications

References 4 publications

The preparation of high purity H235S

The preparation of high purity H235S

Sulfur Compounds

Sulfur Compounds

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Preparation of high purity carbonyl[³⁵S]sulphide

The preparation of high purity H₂³⁵S

The preparation of high purity H₂³⁵S