Preparation of magnetic mesoporous carbon from polystyrene-grafted magnetic nanoparticles for rapid extraction of chlorophenols from water samples

Core‐shell structured magnetic mesoporous carbon nanospheres derived from metal‐polyphenol coordination polymer‐coated Fe3O4 and its application in the enrichment of phthalates from water samples

“…The Fe 3 O 4 MNPs were prepared according to a previously reported solvothermal method with minor modifications , and the Fe 3 O 4 @Fe 3+ ‐TA core‐shell nanospheres were prepared according to a previous report with minor modifications . Briefly, the Fe 3 O 4 MNPs (200 mg) were dispersed in 80 mL of deionized water.…”

“…In recent years, magnetic carbon materials (MCMs) have also been broadly employed in MSPE of trace‐level target species . To date, MCMs are usually fabricated by loading the precursors of magnetic materials onto mesoporous carbon, which are prepared beforehand via hard and soft template‐based methods .…”

“…In addition, the particle size of the metal organic frameworks‐derived MCMs is typically several micrometers, which causes slow mass transfer of the analytes. Nanosized core‐shell structured MCMs can overcome the abovementioned disadvantages, and they have been prepared via carbonization of polymer‐coated magnetic nanoparticles (MNPs) . Nonetheless, these methods are complicated, high‐cost, and time‐consuming.…”

High-efficiency solid-phase microextraction performance of polypyrrole enhanced titania nanoparticles for sensitive determination of polar chlorophenols and triclosan in environmental water samples

“…[6][7][8] Most phenolic compounds are highly toxic, are not very biodegradable, can cause cancer, abnormalities and mutations, and can accumulate in organisms, with potentially serious impacts on the human endocrine system. 9,10 Since the concentration levels of phenolic compounds are generally low in complex matrices, the development of simple, efficient and selective preconcentration and separation techniques for phenolic pollutants in environmental water is highly desirable to achieve reliable results. 11 High-performance liquid chromatography (HPLC) is frequently used to determine phenolic compounds, unlike gas chromatography (GC), it does not lead to the derivatization of compounds.…”

Preparation of magnetic mesoporous composites from glycerol and iron(III) salt

“…Several potential applications of carbon-based magnetic materials have been described in the literature: antibacterial agents; 20 adsorbents of compounds such as phenol and chloroform, 21 textile dyes, 21,22 and metals [cadmium (Cd 2+ ), 23 chromium (Cr 6+ ), 18,[24][25][26][27] arsenic (As 3+ ), 28 and As 5+23,27 etc. Moreover, these materials have been used for the removal of chlorophenol 29 and sulfonamide, 30 degradation or removal of organic compounds, 20,[31][32][33][34] and desulfurization of petroleum. 35…”