2018
DOI: 10.1016/j.ceramint.2018.01.035
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Preparation of presintered zirconia blocks for dental restorations through colloidal dispersion and cold isostatic pressing

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Cited by 19 publications
(8 citation statements)
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“…Cold isostatic pressing is the most common method for compacting ceramic powders. During cold-isostatic pressing, pressure is applied at ambient temperature, gradually increasing from 50 to 400–1000 MPa and transmitted uniformly on zirconia powder until the green compacts reach 40–60% of their theoretical density prior to sintering [26,27]. Factors enhancing the densification and pore elimination during CIP are nano-sized powder particles, uniform particle size distribution, high specific surface area and low degree of agglomeration.…”
Section: Factors Affecting Strength and Aging Resistance Of Monolithimentioning
confidence: 99%
“…Cold isostatic pressing is the most common method for compacting ceramic powders. During cold-isostatic pressing, pressure is applied at ambient temperature, gradually increasing from 50 to 400–1000 MPa and transmitted uniformly on zirconia powder until the green compacts reach 40–60% of their theoretical density prior to sintering [26,27]. Factors enhancing the densification and pore elimination during CIP are nano-sized powder particles, uniform particle size distribution, high specific surface area and low degree of agglomeration.…”
Section: Factors Affecting Strength and Aging Resistance Of Monolithimentioning
confidence: 99%
“…The suspension was constantly magnetically stirred for 15 min to aid the proper mixing of components. The suspension was subsequently placed in an ultrasonic bath for 10 min to break the agglomerates and milled using a Pulverisette-6 (Fritsch, Germany) planetary ball mill at 300 rpm for 120 min, with 10 mm-diameter zirconia balls as grinding media at a ball-to-powder ratio of 10:1 [8].…”
Section: Materials and Methods 21 Materials And Slurry Preparationmentioning
confidence: 99%
“…Amat et al [8] found that the mechanical properties of zirconia block for dental restoration are improved through colloidal and CIP techniques. However, an appropriate presintering temperature that can be used to produce zirconia block with good strength and that can be mounted into jig without damage during machining is not yet completely studied.…”
Section: Introductionmentioning
confidence: 99%
“…By utilizing a special colloidal processing technique, zirconia powder with good particle homogeneity and a packing density of almost 100 wt% can be developed [11]. The combination of wet-processing and slip-casting techniques allows the fabrication of machinable zirconia blocks with good mechanical and aesthetic properties [12][13][14][15]. Furthermore, slip-casted zirconia blocks offer an economical alternative to the traditional compaction process [12] because zirconia slurry can be poured manually into special porous molds (plaster mold) to form zirconia frameworks without the need for specialized machines [13,14].…”
Section: Introductionmentioning
confidence: 99%
“…mm in diameter and 24 mm in length) samples of Zir were fabricated via the colloidal technique and slip-casting process. By using the dispersing technique parameters described by Amat et al[14], a nanozirconia suspension was prepared by mixing nanozirconia powder with distilled water at 1:1.25 weight ratio. Then, 0.5 wt% polyethyleneimine was added to the mixture to disperse the agglomerated zirconia particles, and the suspension pH was adjusted to 2 (Five Easy F20, Mettler Toledo, Swiss) through the addition of hydrochloric solution.…”
mentioning
confidence: 99%