Probing structural features in potato starch granules at moderate hydration through the modelling of 1H-&gt;13C polarization transfer kinetics

Falourd, X.; Lahaye, M.; Rondeau-Mouro, C.

doi:10.1016/j.ijbiomac.2024.132806

International Journal of Biological Macromolecules

2024

DOI: 10.1016/j.ijbiomac.2024.132806

|View full text |Cite

Probing structural features in potato starch granules at moderate hydration through the modelling of 1H->13C polarization transfer kinetics

X. Falourd,

M. Lahaye,

C. Rondeau-Mouro

Help me understand this report

Search citation statements

Order By: Relevance

Paper Sections

Select...

Citation Types

Supporting

Mentioning

Contrasting

Year Published

2024

Publication Types

Select...

Article1

Relationship

Self Cite0

Independent1

Authors

Journals

Cited by 1 publication

References 42 publications

Supporting

Mentioning

Contrasting

Order By: Relevance

A novel approach for quantitative determination of lignin content in tobacco via multiCP/MAS NMR spectroscopy

Wang,

Huang,

Tian

et al. 2024

J Chinese Chemical Soc

View full text Add to dashboard Cite

As the main structural component of tobacco cell wall, lignin content is an important factor affecting the safety of tobacco smoking. However, it is time‐consuming to quantify lignin by conventional wet chemical analysis methods. In this work, a 13C multiCP/MAS NMR spectral analysis method for tobacco lignin was established. The multiCP/MAS NMR sequence was optimized for tobacco lignin. The optimized nuclear magnetic sequence parameters were 9 CP cycles of 1.5 ms, repolarization time of 0.7 s, and a total acquisition time of 130 min. Subsequently, TMSP was used as the internal standard substance to establish the working curve, and the correlation coefficient was 0.9946. The relative standard deviation (RSD, n = 5) was 3.26%. This method was applied to the determination of lignin content in different types of tobacco samples. The relative error in the determination of lignin content by this method did not exceed 4.46% compared to the results of the chemical method. The results showed that the 13C multiCP/MAS NMR spectral analysis method had the advantages of accuracy and rapidity, which provided a new technical means for the quantitative study of tobacco cell wall substances.

show abstract

A novel approach for quantitative determination of lignin content in tobacco via multiCP/MAS NMR spectroscopy

Wang,

Huang,

Tian

et al. 2024

J Chinese Chemical Soc

View full text Add to dashboard Cite

show abstract

scite is a Brooklyn-based organization that helps researchers better discover and understand research articles through Smart Citations–citations that display the context of the citation and describe whether the article provides supporting or contrasting evidence. scite is used by students and researchers from around the world and is funded in part by the National Science Foundation and the National Institute on Drug Abuse of the National Institutes of Health.

Contact Info

customersupport@researchsolutions.com

10624 S. Eastern Ave., Ste. A-614

Henderson, NV 89052, USA

This site is protected by reCAPTCHA and the Google Privacy Policy and Terms of Service apply.

Blog Terms and Conditions API Terms Privacy Policy Contact Cookie Preferences Do Not Sell or Share My Personal Information

Made with 💙 for researchers

Part of the Research Solutions Family.

Probing structural features in potato starch granules at moderate hydration through the modelling of 1H->13C polarization transfer kinetics

Cited by 1 publication

References 42 publications

A novel approach for quantitative determination of lignin content in tobacco via multiCP/MAS NMR spectroscopy

A novel approach for quantitative determination of lignin content in tobacco via multiCP/MAS NMR spectroscopy

Contact Info

Product

Resources

About