Activated carbons were produced from coconut shells of tall and dwarf tree varieties. The activated carbon from the tall tree variety was initially synthesized using 1 M concentration of each of ZnCl 2 , H 3 PO 4 , and KOH solutions. From the adsorptive tests conducted using methylene blue solution, the activated carbon produced with H 3 PO 4 gave the best absorbance and adsorptive performance. Coconut shells of dwarf tree variety were then obtained and treated with same mass of coconut shells of the tall tree variety using varied concentrations of the acid in order to determine whether the optimum concentration and temperature for producing carbon black from the coconut shells are distinct or similar for both varieties. The process was also modelled using the Differential Response Method (DRM) in order to determine the yields and adsorptive performances of the activated carbons by varying the carbonization temperature and concentration. The results from experiment and the developed mathematical model were both found to be in agreement giving the optimum concentration of phosphoric acid and pH for producing activated carbon to be 0.67 M and 2.07 for the tall tree variety and 1 M and 1.98 for the dwarf variety at optimum temperatures in the range of 450-575 ∘ C and 575 ∘ C, respectively.