Pure metallic nanofibrillar membrane for high-performance electrostatic air filtration with antimicrobial and reusable characteristics

As the potential adverse health and environmental effects of nanoscale pollutants have garnered significant attention, the demand for monitoring and capturing ultrafine particulate matter has been growing. With the rise in ultrafine dust emissions, this issue has become increasingly important. However, submicron particles require advanced strategies to be captured because of their limited inertial effect. For example, electrostatic air filters have been investigated for their improved performance in the fine particle regime. On the other hand, Raman spectroscopy was proposed as a promising analytical strategy for aerosol particles because it can be used to conveniently detect analytes in a label-free manner. Thus, the synergistic integration of these strategies can open new applications for addressing environment-related challenges. This study presents a multifunctional approach for achieving both air filtration and surface-enhanced Raman scattering (SERS) for analyte identification. We propose a nanoporous membrane composed of a thin gold layer, copper, and copper oxide to provide the desired functions. The structures are produced by performing scalable electrodeposition and subsequent electron-beam evaporation, attaining an excellent filtration efficiency of 95.9% with an applied voltage of 5 kV for 300 nm KCl particles and a pressure drop of 121 Pa. Raman intensity measurements confirm that the nanodendritic surface of the membrane intensifies the Raman signals and allows for the detection of 10 μL of nanoplastic particle dispersion with a concentration of 50 μg/mL. Rhodamine 6G aerosol stream with an approximate particle deposition rate of 0.040 × 106 mm–2·min–1 is also identified in a minimum detectable time of 50 s. The membrane is shown to be recyclable owing to its structural robustness in organic solvents. In addition, the fatigue resistance of the structure is evaluated through 22,000 iterative loading cycles at a pressure of 177 kPa. No performance degradation is observed after the fatigue loading.

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Material Extrusion 3D Printing of Micro-Porous Copper-Based Structure for Water Filters

Kotorčević,

Milenković,

Živić

et al. 2024

Machines

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This paper presents 3D-printed micro-porous structures made of a Cu/PLA composite by using material extrusion 3D printing technology. A metallic filament made of 80% copper and 20% polylactic acid (PLA) was used for the 3D printing of the porous samples. We varied printing parameters, aiming to obtain a micro-range porosity that can serve as a water-filtering structure. The produced samples were analyzed from the aspects of dimensional accuracy, level of porosity, and capacity for water flow. Several samples were fabricated, and the water flow was exhibited for the samples with an approximate 100 µm size of the interconnected open porosity. The application of material extrusion 3D printing, as a cost-effective, widely available technology for producing micro-range porous structures, is still challenging, especially for interconnected predefined porosity with metal-based filaments. Our research showed that the optimization of 3D printing parameters can enable the fabrication of copper-based micro-porous structures, but further research is still needed.

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Pure metallic nanofibrillar membrane for high-performance electrostatic air filtration with antimicrobial and reusable characteristics

Abstract: Air filters have evolved to satisfy demand for higher air quality in various industries over the decades. The common meltblown polymeric filters have a short lifetime due to charge loss,...

Cited by 3 publications

References 52 publications

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Field-Assisted Efficient Capturing and Analysis of Airborne Nanoparticulate Matter Using a Multifunctional Nanoporous Membrane

Material Extrusion 3D Printing of Micro-Porous Copper-Based Structure for Water Filters

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