Pure shift edited NMR methodologies for the extraction of Homo- and heteronuclear couplings with ultra-high resolution

Mishra, Saket; Suryaprakash, N.

doi:10.1016/j.pnmrs.2023.02.001

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Cited by 4 publications

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“…Resolution is increased by dispersing signals into a second frequency dimension, but additional time is required to sample this dimension -several hours where high digital resolution is required to overcome signal overlap. 2D pure shift NMR experiments [5][6][7][8] can reduce the time needed to sample the second dimension by suppressing signal multiplicity. These methods provide clear and simple correlations, but reduce the chemical information content of the spectrum, and almost always incur a sensitivity penalty.…”

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confidence: 99%

Ultra-selective 1D clean in-phase correlation spectroscopy

et al. 2023

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confidence: 99%

Ultra-selective 1D clean in-phase correlation spectroscopy

et al. 2023

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N-heterocyclic carbene promoted one-pot synthesis of 1,2-diols and ɑ-Hydroxyketones from simple aldehydes

Cao,

Liu,

et al. 2024

Molecular Catalysis

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NMR spectroscopy of small molecules in solution

Nolis

2024

Nuclear Magnetic Resonance

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This book chapter covers relevant articles published in peer-reviewed journals in 2023 in the field of NMR spectroscopy of small molecules in solution. Articles appeared in 2023 as accepted online versions but not published until 2024 are not included. The chapter is structured into seven sections: NMR pulse sequence development, structural determination in oriented media, mixture analysis, quantitative NMR, NMR chiral recognition methodologies, artificial intelligence methods and a final miscellanea section where interesting articles that did not fit in any of the earlier topics were embedded. Noticeably, many articles could fit in more than one section, since most of the topics are intimately related. The reader should not expect a fully detailed review, nor a simple, non-detailed listing of articles. Instead, the reader shall find distilled information with description of the key points and the main goals.

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Pure shift edited NMR methodologies for the extraction of Homo- and heteronuclear couplings with ultra-high resolution

Cited by 4 publications

References 148 publications

Ultra-selective 1D clean in-phase correlation spectroscopy

Ultra-selective 1D clean in-phase correlation spectroscopy

N-heterocyclic carbene promoted one-pot synthesis of 1,2-diols and ɑ-Hydroxyketones from simple aldehydes

NMR spectroscopy of small molecules in solution

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