Purity of Boron Produced by the Decomposition of Diborane and Subsequent Zone-Melting

Hinz, Ingeborg; Wirth, Heinz

doi:10.1007/978-1-4899-6574-5_2

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B) Decomposition Of Boron Hydrides1

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1977

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“…Decomposition is carried out by passing a gaseous hydride, usually diluted with hydrogen, through the heated quartz tube. Similar results were also obtained by heating solid boron hydrides at 800-900 o C in a small boat (made of boron nitride) • Pyrolysis on an incandescent tungsten and tantalum (WIRTH and DIETZE, 1964;HINZ and WIRTH, 1965) filament results in formation of boron rods or films (SCHRANGLE and DIETZE, 1972) with crystalline structure.…”

Section: B) Decomposition Of Boron Hydridessupporting

confidence: 62%