“…1f,g [α] 26 D = +1.7° (c = 1.0, CHCl3), white solid, Mp. 58-59 °C, δH(CDCl3) 1.00 (3H, s), 1.13 (3H, s), 3.73 (1H, dd, J 4.2, 11.5 Hz), 3.79 (3H,s),4.66 (1H,dd,J 4.2,12.8 Hz),4.81 (1H,dd,J 11.5,12.8 Hz),6.86 (2H,d,J 8.7 Hz),7.11 (2H,d,J 8.7 Hz), 9.53 (1H, s); δC(CDCl3) 18.7, 21.4, 47.7, 48.2, 55.1, 76.4, 113.9, 126.9, 130.0, 159.2, 204.3; ν(KBr)/cm -1 2976,2919,2841,2718,1725,1611,1582,1553,1516,1468,1441,1379,1290,1250,1188,1119,1028,889,839,812,747,635 8, 21.6, 47.8, 48.0, 75.9, 122.1, 130.6, 131.8, 134.3, 203.7; ν(KBr)/cm -1 3030,2973,2934,2874,2818,2718,1728,1559,1487,1468,1441,1410,1381,1350,1306,…”