Quantification of Allantoin in Yams (<i>Dioscorea</i> sp.) Using a <sup>1</sup>H NMR Spectroscopic Method

Cao, Thao Quyen; Hahn, Dongyup

doi:10.4014/jmb.2301.01009

Cited by 4 publications

(1 citation statement)

References 32 publications

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“…The samples for evaluation of intra-and interday precision could be either one plant extract sample (Cao and Hahn, 2023) or one standard sample (Windarsih et al, 2018;Thongphichai et al, 2022) (e.g., samples from linearity test). It is important to carry out 1 H qNMR experiments along the day (repeatability/intraday precision) and on non-sequential alternate days (reproducibility/ interday precision).…”

Section: Qnmr Validationmentioning

confidence: 99%

qNMR in natural products: practical approaches. What nobody tells you before starting your qNMR study!

Ravaglia,

de Oliveira,

Holzgrabe

et al. 2024

Front. Nat. Prod.

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NMR (Nuclear Magnetic Resonance) spectroscopy is a well-established technique for elucidating the structure and composition of Natural Products (NP). However, while NMR spectra offer qualitative insights, there is often a growing demand within the NP research community for quantitative analysis using NMR techniques. Unfortunately, this demand is sometimes met with misconceptions and lacks the methodological rigor typically associated with analytical procedures, particularly concerning validation and mandatory adjustments of quantitative NMR (qNMR) parameters. Therefore, this minireview highlights the practical approaches concerning preparation and validation for qNMR analyses of plant extracts. Specifically, we provide a concise protocol detailing experimental settings crucial for ensuring the accuracy and reliability of quantitative measurements. It is noteworthy that such guidance is often absent in existing literature, and our minireview wants to bridge this gap by offering clear methodological recommendations.

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Section: Qnmr Validationmentioning

confidence: 99%

qNMR in natural products: practical approaches. What nobody tells you before starting your qNMR study!

Ravaglia,

de Oliveira,

Holzgrabe

et al. 2024

Front. Nat. Prod.

View full text Add to dashboard Cite

show abstract

The lesser yam Dioscorea esculenta (Lour.) Burkill: a neglected crop with high functional food potential

Lebot,

Abraham,

Melteras

2024

Genet Resour Crop Evol

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Chemical Composition of Spheciospongia Aff. Mastoidea Sponge from the Red Sea and Uses of Its Polysaccharides in the Biosynthesis of Silver Nanoparticles with Antimicrobial and Anticancer Activity

Eltanany,

Faraag,

Ebrahim

et al. 2024

Thalassas

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Quantification of Allantoin in Yams (Dioscorea sp.) Using a ¹H NMR Spectroscopic Method

Cited by 4 publications

References 32 publications

qNMR in natural products: practical approaches. What nobody tells you before starting your qNMR study!

qNMR in natural products: practical approaches. What nobody tells you before starting your qNMR study!

The lesser yam Dioscorea esculenta (Lour.) Burkill: a neglected crop with high functional food potential

Chemical Composition of Spheciospongia Aff. Mastoidea Sponge from the Red Sea and Uses of Its Polysaccharides in the Biosynthesis of Silver Nanoparticles with Antimicrobial and Anticancer Activity

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Quantification of Allantoin in Yams (Dioscorea sp.) Using a 1H NMR Spectroscopic Method

Cited by 4 publications

References 32 publications

qNMR in natural products: practical approaches. What nobody tells you before starting your qNMR study!

qNMR in natural products: practical approaches. What nobody tells you before starting your qNMR study!

The lesser yam Dioscorea esculenta (Lour.) Burkill: a neglected crop with high functional food potential

Chemical Composition of Spheciospongia Aff. Mastoidea Sponge from the Red Sea and Uses of Its Polysaccharides in the Biosynthesis of Silver Nanoparticles with Antimicrobial and Anticancer Activity

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Product

Resources

About

Quantification of Allantoin in Yams (Dioscorea sp.) Using a ¹H NMR Spectroscopic Method