Quick setting plug for capillary column making

Cueman, M. Kent

doi:10.1002/jhrc.1240010203

Cited by 13 publications

(3 citation statements)

References 3 publications

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“…The recently developed immobilized stationary phases for glass OTCs have received considerable attention [341][342][343][344][345][346][347][348] and it appears that these types of phases will be used extensively in the future. Along with these advances, there have been several new procedures [349][350][351][352][353][354] for sealing the filled tube prior to removing the volatile solvent. These sealing techniques have made it possible to increase the reproducibility of column preparation.…”

Section: Brief Description Of Techniques For Preparing Various Types mentioning

confidence: 99%

Aspects of High-Resolution Gas Chromatography as Applied to the Analysis of Hydrocarbon Fuels and Other Complex Organic Mixtures. Volume 1

Rubey¹

1985

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Symmetric elution zone profile 3 Partially disengaged solute zones 4 Block diagram of basic systems approach 5 Three general forms of Chromatographie zone profiles Ig 6 Different combinations of solute zone profiles. 17 7 Rapidly generated chromatogram of a jet fuel. . 8 Chromatogram of a jet fuel obtained with a Pyrex glass open tubular column 9 Gaussian and exponentially modified Gaussian elution zone profiles 10 Series of normal paraffins eluted from a contaminated column 11 Elution behavior after removing contaminated section of column 12 Open tubular column gas chromatograms that exhibit unusual baseline behavior 13 Undesirable quantitative behavior 41 14 Relationship of three-component gas Chromatographie compromises 4 3 15 Relationship of admitted solute versus solute zone variance 44 16 Graphic procedures for measuring solute zone asymmetry 4 6

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Section: Brief Description Of Techniques For Preparing Various Types mentioning

confidence: 99%

Aspects of High-Resolution Gas Chromatography as Applied to the Analysis of Hydrocarbon Fuels and Other Complex Organic Mixtures. Volume 1

Rubey¹

1985

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“…Moreover, in a humid environment, even an overnight period cannot assure perfect plug closure, because the dried silicate swells again under the action of ambient water and looses its tightness. Faster and more durable closures could be made by using alternative substances, such as epoxy glue [5], self-curing silicone rubber [6], or vinyl monomer (methyl methacrylate) polymerization induced by peroxides and UV light [7].…”

Section: Introductionmentioning

confidence: 99%

End Closures for Fused Silica and Glass Capillary GC Columns

Nardi

1998

J. High Resol. Chromatogr.

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“…In recent years different methods of sealing have been described, for example by means of water glass [l], epoxy glue [2] or a stopper [3]. In our opinion a lot of experience is necessary if these techniques are to be successfully applied.…”

Section: Introductionmentioning

confidence: 99%