The radiation induced optical absorption in Perspex ' Red 400 ' manufactured hy Imperial Chemical Industries Limited, has been investigated with reference to its use in the dosimetry of high doses of ionizing radiation. It is found that this Perspex can he divided into three distinct types, each having a particular dyestuff formulation. The type currently available commercially exhibits two peaks in the induced absorption spectrum, at 613 mp and 394 mp. The highest extinction coefficient is obtained by measuring at 394 mp with a spectrophotometer, in n-hich case the optical density change in 0.15 cm thick samples is a linear function of dose between 0.2 and 1.5 nn-ad. A method has bcen developed which requires only a simple white light photometer with suitable optical filtration, with a reduction in sensitivity of not more than 50O;.