Radiation synthesis of poly(2-vinylpyridine) gels and their swelling characteristics

Acar, Nermin

doi:10.1016/s0969-806x(01)00231-6

Cited by 15 publications

(8 citation statements)

References 28 publications

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“…The bags prepared from filter paper were used to determine swelling properties of the crosslinked polymers 53. First, the bags were immersed in the solvent and blotted quickly with an absorbent paper; this was followed by addition of a dried polymer sample of known weight into the bags.…”

Section: Methodsmentioning

confidence: 99%

Novel poly(orthosilicate)s based on linear aliphatic diols: Synthesis, characterization, and swelling properties

Karadag

Sönmez

2013

J of Applied Polymer Sci

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Condensation reactions between tetraethyl orthosilicate and linear aliphatic diol monomers at moderately high temperatures in proper stoichiometric ratios gave crosslinked poly(orthosilicate)s. The synthesized crosslinked polymers were found to be insoluble in common organic solvents, such as tetrahydrofuran, dichloromethane, benzene, and acetone, but did show swelling abilities in these solvents. All of the crosslinked polymers had moderate thermal stability and good, regenerable solvent uptake abilities. The synthesized polymers have been characterized by Fourier transform infrared spectroscopy solid-state 13 C-and 29 Si-NMR, thermogravimetric analysis, differential scanning calorimetry methods, and elemental analysis. In this report, the synthesis characterization, and swelling properties of crosslinked poly(orthosilicate)s for environmental removal and recovery of organic solvents are presented. The effect of the length of the aliphatic diol monomers on the properties of the synthesized polymers was also examined.

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Section: Methodsmentioning

confidence: 99%

Novel poly(orthosilicate)s based on linear aliphatic diols: Synthesis, characterization, and swelling properties

Karadag

Sönmez

2013

J of Applied Polymer Sci

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“…To determine the swelling properties of the crosslinked polymers, bags prepared from filter paper were employed. 53 The bags were first immersed in the solvent and blotted quickly with an absorbent paper; then, a dried polymer sample of known weight was added into the bags. The filled bags were immersed in the solvent.…”

Section: Methodsmentioning

confidence: 99%

Synthesis and swelling properties of crosslinked poly(orthosilicate)s from cyclohexanedimethanols

Sönmez

Karadag

Onaran

2011

J of Applied Polymer Sci

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Condensations of cyclohexanedimethanol derivatives with tetraethyl orthosilicate in the proper stoichiometric ratio produce crosslinked poly(orthosilicate)s. Synthesized crosslinked polymers have swelling abilities in common organic solvents such as tetrahydrofuran (THF), dichloromethane, benzene and acetone. All these polymers are moderately thermally stable and possess solvent uptake abilities that are not only good and fast but are also regen-erable. FTIR, solid-state 13 C, 29 Si-NMR and thermal methods were used to characterize these synthesized polymers. The effects of different cyclohexanedimethanol derivatives on the properties of polymers were also examined.

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“…Bags prepared from filter paper were used to calculate the swelling properties of the cross-linked polymers (Acar, 2002). First, the bags were immersed in the solvent and blotted quickly with absorbent paper; this was followed by the addition of a dried polymer sample of known weight into the bags.…”

Section: Swelling Testsmentioning

confidence: 99%

Poly(alkoxysilane) reusable organogels for removal of oil/organic solvents from water surface

Kizil

Karadag

Aydin

et al. 2015

Journal of Environmental Management

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Radiation synthesis of poly(2-vinylpyridine) gels and their swelling characteristics

Cited by 15 publications

References 28 publications

Novel poly(orthosilicate)s based on linear aliphatic diols: Synthesis, characterization, and swelling properties

Novel poly(orthosilicate)s based on linear aliphatic diols: Synthesis, characterization, and swelling properties

Synthesis and swelling properties of crosslinked poly(orthosilicate)s from cyclohexanedimethanols

Poly(alkoxysilane) reusable organogels for removal of oil/organic solvents from water surface

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