Rapid synthesis of mesoporous silica by an accelerated microwave radiation method

Song, M.; Kim, Jong-Yun; Cho, Sung-Ho; Kim, Jong-Duk

doi:10.1007/bf02719498

Cited by 7 publications

(2 citation statements)

References 41 publications

Supporting

Mentioning

Contrasting

Order By: Relevance

“…Employing microwave‐assisted procedures permits a fine‐tuning of synthesis time and temperature that affect silica condensation rate, template behavior and consequently structural, and textural properties of as‐obtained OMSs. [ 24–34 ] The physicochemical characterization of the exemplary MCM‐41 and SBA‐15 obtained by microwave‐assisted methods is shown in Figure . For example, Ergün et al.…”

Section: Microwave Synthesis Of Nanoporous Materials and Their Applicationsmentioning

confidence: 99%

See 1 more Smart Citation

Advances in Microwave Synthesis of Nanoporous Materials

et al. 2021

View full text Add to dashboard Cite

Usually, porous materials are synthesized by using conventional electric heating, which can be energy‐ and time‐consuming. Microwave heating is commonly used in many households to quickly heat food. Microwave ovens can also be used as powerful devices in the synthesis of various porous materials. The microwave‐assisted synthesis offers a simple, fast, efficient, and economic way to obtain many of the advanced nanomaterials. This review summarizes the recent achievements in the microwave‐assisted synthesis of diverse groups of nanoporous materials including silicas, carbons, metal–organic frameworks, and metal oxides. Microwave‐assisted methods afford highly porous materials with high specific surface areas (SSAs), e.g., activated carbons with SSA ≈3100 m2 g−1, metal–organic frameworks with SSA ≈4200 m2 g−1, covalent organic frameworks with SSA ≈2900 m2 g−1, and metal oxides with relatively small SSA ≈300 m2 g−1. These methods are also successfully implemented for the preparation of ordered mesoporous silicas and carbons as well as spherically shaped nanomaterials. Most of the nanoporous materials obtained under microwave irradiation show potential applications in gas adsorption, water treatment, catalysis, energy storage, and drug delivery, among others.

show abstract

Section: Microwave Synthesis Of Nanoporous Materials and Their Applicationsmentioning

confidence: 99%

“…Porous silicas obtained via microwave‐assisted methods with their SSA, and potential applications are summarized in Table 3 . [ 24–63 ]…”

Section: Microwave Synthesis Of Nanoporous Materials and Their Applicationsmentioning

confidence: 99%