Recent developments in flow-injection atomic spectroscopy

Castro, M. D. Luque de; Gámiz‐Gracia, Laura

doi:10.1016/s1068-5561(98)80006-4

Cited by 5 publications

(3 citation statements)

References 190 publications

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“…and AAS, [10] as well as flow injection analysis. [11] A major reason that few major developments have occurred in AAS in the last few decades is because it has matured as an analytical technique and for many applications 'it works'.…”

Section: Recent Developments In Atomic Absorption Spectrometrymentioning

confidence: 99%

Recent Applications of Flame Atomic Absorption Spectrometry to Environmental Measurements

Janusa

Beck

2002

Applied Spectroscopy Reviews

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Section: Recent Developments In Atomic Absorption Spectrometrymentioning

confidence: 99%

Recent Applications of Flame Atomic Absorption Spectrometry to Environmental Measurements

Janusa

Beck

2002

Applied Spectroscopy Reviews

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“…[2][3][4][5][6] The advantages of the combination of FI on-line preconcentration with spectrometry have been reviewed in the previous paper. 7 Various adsorbents have so far been reported for the on-line preconcentration of lead (and other heavy metals) in water samples.…”

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On-line Preconcentration and Determination of Traces of Lead in River-water and Seawater by Flow Injection-Flame Atomic Absorption Spectrometry and ICP-Mass Spectrometry

2002

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“…[4][5][6][7] In this respect, FI systems combined with ion exchange or solid phase extraction techniques carried out in minicolumns have been successfully used in flame atomic absorption spectrometry (FAAS) because the preconcentrated analytes can be simply eluted into the nebulizer. [5][6][7][8] A large variety of highly efficient sorbents are usually used in on-line techniques for determination of trace metals, as reviewed by Yebra-Biurrum. 9 These sorbents include inorganic activated alumina; ion exchangers modified with complexing reagents; sorbents based on silica gel, naphthalene, styrenedivinylbenzene copolymers (XAD), and porous glass beads with immobilized chelates groups; reversed-phase silica sorbent (C18, C16 and C8); activated carbon; and chelating resins and celluloses.…”

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On-line Preconcentration and Determination of Lead in Iron and Steel by Flow Injection-Flame Atomic Absorption Spectrometry

et al. 2000

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High purity iron has recently received much attention as a new material with excellent characteristics. 1,2 The development of reliable analytical methods for the determination of trace impurity elements are required for production of pure iron. On the other hand, the use of scrap iron is increasing to make use of resources effectively and the accurate determination of various impurity metals in iron and steel is therefore essential for the quality control of iron products.The detection limit of lead by flame atomic absorption spectrometry (FAAS) is about 10 ng/ml. 3 Therefore the determination of traces of lead in high purity metals by FAAS usually requires its preconcentration, in addition to the separation of lead from matrix elements. Generally the blank value introduced from the reagents or from the laboratory environment must be kept at as low a level as possible in order to obtain the precise analytical results for traces of lead.Flow injection (FI) on-line preconcentration procedures now play an important role in trace metal analysis. They offer the possibility of determining lower analyte concentrations and avoiding matrix effects by separation of the analyte from interfering matrix components. Furthermore the consumption of time, sample and reagent, and the risk of contamination from the laboratory environment are low; the repeatability and efficiency are high compared with its corresponding batch counterpart procedures. [4][5][6][7] In this respect, FI systems combined with ion exchange or solid phase extraction techniques carried out in minicolumns have been successfully used in flame atomic absorption spectrometry (FAAS) because the preconcentrated analytes can be simply eluted into the nebulizer. [5][6][7][8] A large variety of highly efficient sorbents are usually used in on-line techniques for determination of trace metals, as reviewed by Yebra-Biurrum. 9 These sorbents include inorganic activated alumina; ion exchangers modified with complexing reagents; sorbents based on silica gel, naphthalene, styrenedivinylbenzene copolymers (XAD), and porous glass beads with immobilized chelates groups; reversed-phase silica sorbent (C18, C16 and C8); activated carbon; and chelating resins and celluloses. The typical chelating resin, Chelex-100, with iminodiacetate chelating groups has been among the most used. These sorbents are mostly used for determination of trace metal ions in natural water, biological samples, and food, but in some cases, these samples bring about difficulties if they contain large amounts of metal ions. For example, this problem gets complicated when trace elements are determined in complex metallic matrix samples such as waste water, alloys and rocks, because the column adsorbs not only micro components but also some matrix elements like iron, copper and others as well, and the sorbent capacity is insufficient.This work was undertaken to examine a Pb-selective chromatographic resin, 10 Pb·Spec TM (EIChrom Industries), to preconcentrate and separate lead from other sample matrix comp...

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Recent developments in flow-injection atomic spectroscopy

Cited by 5 publications

References 190 publications

Recent Applications of Flame Atomic Absorption Spectrometry to Environmental Measurements

Recent Applications of Flame Atomic Absorption Spectrometry to Environmental Measurements

On-line Preconcentration and Determination of Traces of Lead in River-water and Seawater by Flow Injection-Flame Atomic Absorption Spectrometry and ICP-Mass Spectrometry

On-line Preconcentration and Determination of Lead in Iron and Steel by Flow Injection-Flame Atomic Absorption Spectrometry

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