Recent Trends in the Synthesis of Linear Peptides

Kapoor, A.

doi:10.1002/jps.2600590102

Journal of Pharmaceutical Sciences

1970

DOI: 10.1002/jps.2600590102

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Recent Trends in the Synthesis of Linear Peptides

A. Kapoor

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1970

1979

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Cited by 6 publications

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ChemInform Abstract: NEUE SYNTH. VON LINEAREN PEPTIDEN

Kapoor¹

1970

Chemischer Informationsdienst. Organische Chemie

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Nach einer Übersicht über die gebräuchlichen Schutzgruppen für die Amin und Esterfunktion, ihre Anwendbarkeit und Problematik werden die klassischen und modernen Methoden für die Knüpfung einer Peptidbindung abgehandelt unter besonderer Berücksichtigung polymerer Trägersubstanzen, mit deren Hilfe die Isolierung und Reinigung der Kupplungsprodukte nahezu ohne Racemisierung oft besonders leicht gelingt.

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ChemInform Abstract: NEUE SYNTH. VON LINEAREN PEPTIDEN

Kapoor¹

1970

Chemischer Informationsdienst. Organische Chemie

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Thermal decomposition of s‐2‐benzothiazole thiocarbonates

Chen

1976

Journal of Heterocyclic Chem

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Thermal decompositions of S‐2‐benzothiazole thiocarbonates have been investigated. The results are best rationalized by an Sni ion‐pair return mechanism from which S‐substituted benzothiazoles are the major products obtained. The ready ionization of the carbon‐oxygen bond of thiocarbonates at elevated temperature renders a concerted Sni mechanism (internal substitution with allylic rearrangement) inoperative. Of particular interest is the mixed benzo‐thiazole‐2‐thiol and 2‐thione compound isolated from the decomposition of 2 (or 3)‐halogen‐substituted ethyl (or propyl) thiocarbonates. Evidence is presented that the thione 14 results from the nucleophilic opening of the cyclic intermediate, 2,3‐dihydrothiazolo[2,3‐b]benzothi‐azolium chloride (20). The latter is readily formed under the experimental condition by intramolecular cyclization of the corresponding 2‐(2‐chloroethyl)benzothiazole (23), a primary product from the decomposition of S‐2‐benzothiazole 2‐chloroethylthiocarbonate (7).

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Synthesis of Cyclic Peptides

Kopple

1972

Journal of Pharmaceutical Sciences

103

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Recent Trends in the Synthesis of Linear Peptides

Cited by 6 publications

References 177 publications

ChemInform Abstract: NEUE SYNTH. VON LINEAREN PEPTIDEN

ChemInform Abstract: NEUE SYNTH. VON LINEAREN PEPTIDEN

Thermal decomposition of s‐2‐benzothiazole thiocarbonates

Synthesis of Cyclic Peptides

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