Laminated glass is ever more frequently used nowadays. This applies to the automobile industry and the construction industry. In cars, this refers mostly to the front and rear windows, whereas in construction, technical safety glass is used for railings and window glass. The task of this type of glass is to provide sufficient resistance against mechanical impact and unpleasant weather conditions. At the same time, if it is damaged, it has to break into the smallest possible pieces, or, wherever possible, the glass should remain intact on the interlayer film to prevent shards from injuring people and animals in the immediate vicinity. The paper deals with the recycling of laminated glass, especially with the effective separation of glass (in the form of cullet) from the polyvinyl butyral (PVB) interlayer film. The experimental research is focused on the mechanical separation of glass from the interlayer film by vibration, and also on the chemical cleaning of PVB film in order to allow subsequent recycling of both materials. The results quantify the efficiency of mechanical separation in the form of weight loss of the sample of laminated glass and define the particle size distribution of glass cullet, which is an important parameter in the possibility of glass recycling. The research leads to a methodology proposal for the separation of glass and PVB film and the design of equipment for this method.