2023
DOI: 10.1002/chem.202300933
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Regioselective Dehydrogenative Reverse Prenylation of Indoles with 2‐Methyl‐2‐butene

Abstract: Bulk chemical 2-methyl-2-butene, one of the main C5 distillates of the petrochemical industry, has scarcely been utilized directly in synthesizing high-value-added fine chemicals. Herein, we use 2-methyl-2-butene as the starting material to develop a palladium-catalyzed highly site-and regio-selective C-3 dehydrogenation reverse prenylation of indoles. This synthetic method features mild reaction conditions, a broad substrate scope, atom-and step-economies.

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